Technology Process of Copper, [1,2,3,4,8,9,10,11,15,16,17,18,22,23,24,25-hexadecachloro-29H,31H-phthalocyaninato(2-)-kappaN29,kappaN30,kappaN31,kappaN32]-, (SP-4-1)-
There total 6 articles about Copper, [1,2,3,4,8,9,10,11,15,16,17,18,22,23,24,25-hexadecachloro-29H,31H-phthalocyaninato(2-)-kappaN29,kappaN30,kappaN31,kappaN32]-, (SP-4-1)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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In
neat (no solvent);
chlorination of (CuC32H8Cl8N8) in presence of freshly recrystd. Sb2S3 at 200-210°C;;
- Guidance literature:
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ammonium molybdate;
In
further solvent(s);
tetrachloro-phthalic acid anhydride, urea and CuCl in the diluent polychlorobenzene or trichlorobenzene in the presence of (NH4)2MoO4 as catalyst; various temp.;; impurities: chlorphthalocyanine;;
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12775-96-1,15158-11-9,15721-63-8,16941-75-6,17493-86-6,19498-52-3,20499-83-6,20499-84-7,20499-85-8,20499-86-9,20573-10-8,20573-11-9,21595-51-7,21595-52-8,22206-52-6,26445-28-3,28959-95-7,37362-93-9,39417-05-5,54603-16-6,54603-23-5,54603-32-6,54603-40-6,54603-48-4,54603-81-5,54603-89-3,56316-56-4,95985-91-4,122297-32-9,7440-50-8
copper
- Guidance literature:
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arsenic(V) oxide;
In
nitrobenzene;
tetrachloro-phthalic acid anhydride, urea and Cu in the diluent nitrobenzene in the presence of As2O5 as catalyst;; impurities: chlorphthalocyanine;;