Technology Process of N-(2,3-dimethyl-6-methoxyphenyl)acetamide
There total 4 articles about N-(2,3-dimethyl-6-methoxyphenyl)acetamide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine;
In
tetrahydrofuran;
for 3h;
Ambient temperature;
DOI:10.1021/jo970388p
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 86 percent / NaNO3, conc. HCl, acetic anhydride / diethyl ether; CH2Cl2 / 0.25 h / Ambient temperature
2: 100 percent / potassium carbonate / dimethylformamide / 4.5 h / Ambient temperature
3: 80 percent / H2, acetic acid / Pd/C / ethanol / 8 h / 3102.9 Torr / Ambient temperature
4: 92 percent / triethylamine / tetrahydrofuran / 3 h / Ambient temperature
With
hydrogenchloride; sodium nitrate; hydrogen; acetic anhydride; potassium carbonate; acetic acid; triethylamine;
palladium on activated charcoal;
In
tetrahydrofuran; diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo970388p
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 100 percent / potassium carbonate / dimethylformamide / 4.5 h / Ambient temperature
2: 80 percent / H2, acetic acid / Pd/C / ethanol / 8 h / 3102.9 Torr / Ambient temperature
3: 92 percent / triethylamine / tetrahydrofuran / 3 h / Ambient temperature
With
hydrogen; potassium carbonate; acetic acid; triethylamine;
palladium on activated charcoal;
In
tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jo970388p