Cyclohexen-3-ylglycine

Base Information

• Chemical Name: Cyclohexen-3-ylglycine
• CAS No.: 23364-04-7
• Molecular Formula: C8H13NO2
• Molecular Weight: 155.197
• Hs Code.: 2922499990
• European Community (EC) Number: 245-614-1
• DSSTox Substance ID: DTXSID40946034
• Nikkaji Number: J77.845A
• Mol file: 23364-04-7.mol

Synonyms:Cyclohexen-3-ylglycine;23364-04-7;3-Cyclohexenylglycine;BRN 2831205;EINECS 245-614-1;alpha-Aminocyclohex-3-ene-1-acetic acid;3-Cyclohexene-1-acetic acid, alpha-amino-;2-amino-2-(cyclohex-3-en-1-yl)acetic acid;Cyclohex-3-ene-1-acetic acid, alpha-amino-;2-amino-2-cyclohex-3-en-1-ylacetic acid;Amino-cyclohex-3-enyl-acetic acid;Aminocyclohex-3-enylacetic acid;SCHEMBL11686516;Aminocyclohex-3-enyl-acetic acid;DTXSID40946034;AKOS009808159;AMINO-CYCLOHEX-3-ENYL-ACETICACID;2-amino-2-(cyclohex-3-enyl)acetic acid;alpha-Amino-3-cyclohexene-1-acetic acid;LS-57384;FT-0694829;AMINO(CYCLOHEX-3-EN-1-YL)ACETIC ACID;EN300-1261826

Chemical Property of Cyclohexen-3-ylglycine

Chemical Property:

• Vapor Pressure: 0.000389mmHg at 25°C
• Refractive Index: 1.534
• Boiling Point: 294.7 °C at 760 mmHg
• Flash Point: 132 °C
• PSA: 63.32000
• Density: 1.161 g/cm³
• LogP: 1.45490
• XLogP3: -1.6
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 155.094628657
• Heavy Atom Count: 11
• Complexity: 177

Purity/Quality:

99%, ^*data from raw suppliers

AMINO-CYCLOHEX-3-ENYL-ACETIC ACID 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CC(CC=C1)C(C(=O)O)N

Technology Process of Cyclohexen-3-ylglycine

There total 2 articles about Cyclohexen-3-ylglycine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-(cyclohex-3-en-1-yl)imidazolidine-2,4-dione (58668-81-8) → amino-cyclohex-3-enyl-acetic acid (23364-04-7)

Guidance literature:

With barium dihydroxide;

DOI:10.1021/ja01544a028

Reference yield:

3-Cyclohexene-1-carboxaldehyde (100-50-5,61746-36-9) → amino-cyclohex-3-enyl-acetic acid (23364-04-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 4>2CO₃; KCN; aqueous ethanol

2: aqueous Ba(OH)2

With potassium cyanide; barium dihydroxide; ethanol; ammonium carbonate;

DOI:10.1021/ja01544a028

upstream raw materials:

5-(cyclohex-3-en-1-yl)imidazolidine-2,4-dione

3-Cyclohexene-1-carboxaldehyde