Technology Process of 2-(2-chlorophenyl)-2-(6,7-dihydrothieno[3,2-c]pyridin-5(4H)-yl)acetaldehyde
There total 3 articles about 2-(2-chlorophenyl)-2-(6,7-dihydrothieno[3,2-c]pyridin-5(4H)-yl)acetaldehyde which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridinium chlorochromate;
In
dichloromethane;
at 20 - 40 ℃;
for 8h;
Celite;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium carbonate / water
1.2: 1 h / 0 - 20 °C
2.1: pyridinium chlorochromate / dichloromethane / 8 h / 20 - 40 °C / Celite
With
sodium carbonate; pyridinium chlorochromate;
In
dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: diisobutylaluminium hydride / dichloromethane; hexane / 1 h / 20 °C
2: pyridinium chlorochromate / dichloromethane / 8 h / 20 - 40 °C
With
diisobutylaluminium hydride; pyridinium chlorochromate;
In
hexane; dichloromethane;