dimethyl antimony ⁽³⁺⁾; tris chloride

Base Information

• Chemical Name: dimethyl antimony ⁽³⁺⁾; tris chloride
• CAS No.: 7289-79-4
• Molecular Formula: C₂H₆Cl₃Sb
• Molecular Weight: 258.179
• Mol file: 7289-79-4.mol

Synonyms:dimethyl antimony ⁽³⁺⁾; tris chloride

Chemical Property of dimethyl antimony ⁽³⁺⁾; tris chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of dimethyl antimony ⁽³⁺⁾; tris chloride

There total 2 articles about dimethyl antimony ⁽³⁺⁾; tris chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

antimonypentachloride (7647-18-9) + tetramethylstannane (594-27-4) → dimethyltin dichloride (753-73-1) + dimethyl antimony (3+); tris chloride (7289-79-4)

Guidance literature:

In neat (no solvent); SbCl5 was added dripwise; N2 atm., NMR tube; evapn. in vac.;

DOI:10.1016/S0277-5387(00)84652-5

Reference yield:

trimethyltin(IV)chloride (1066-45-1) + antimonypentachloride (7647-18-9) → dimethyltin dichloride (753-73-1) + dimethyl antimony (3+); tris chloride (7289-79-4)

Guidance literature:

In neat (no solvent); SbCl5 was added dropwise; N2 atm., NMR tube;

DOI:10.1016/S0277-5387(00)84652-5

Reference yield: 85.0%

tetraphenylstibonium bromide (16894-69-2,21450-52-2) + dimethyl antimony (3+); tris chloride (7289-79-4) + diphenylantimony trichloride (21907-22-2) → (C6H5)4Sb(1+)*Sb(C6H5)2BrCl3(1-)=[(C6H5)4Sb][Sb(C6H5)2BrCl3] (75577-07-0)

Guidance literature:

In methanol; soln. of Ph4SbBr in MeOH added dropwise to Ph2SbCl3 in MeOH, stirred for1 h at room temp.; solvnet removed in vac., recrystd. from MeCN; elem. anal.;

DOI:10.1016/j.jorganchem.2010.02.016

upstream raw materials:

antimonypentachloride

tetramethylstannane

trimethyltin(IV)chloride

Downstream raw materials:

methylene chloride

methylantimondichloride

(C₆H₅)4Sb⁽¹⁺⁾*Sb(C₆H₅)2BrCl₃^(1-)=[(C₆H₅)4Sb][Sb(C₆H₅)2BrCl₃]

[Ph₄P][Me₂SbCl₄]