PYRIMIDINE N-OXIDE, 97%

Base Information

• Chemical Name: PYRIMIDINE N-OXIDE, 97%
• CAS No.: 17043-94-6
• Molecular Formula: C4H4N2O
• Molecular Weight: 96.0886
• Mol file: 17043-94-6.mol

Synonyms:PYRIMIDINE N-OXIDE, 97%;Pyrimidine, 1-oxide (6CI,7CI,8CI,9CI);Pyrimidine-1-oxide

Chemical Property of PYRIMIDINE N-OXIDE, 97%

Chemical Property:

• Vapor Pressure: 0.0553mmHg at 25°C
• Melting Point: 90-94 °C
• Refractive Index: 1.564
• Boiling Point: 241.6 °C at 760 mmHg
• Flash Point: 99.9 °C
• PSA: 38.35000
• Density: 1.19 g/cm³
• LogP: 0.51010

Purity/Quality:

98%,99%, ^*data from raw suppliers

Pyrimidine N-oxide 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xn
• Hazard Codes: Xn
• Statements: 22-36
• Safety Statements: 26

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of PYRIMIDINE N-OXIDE, 97%

There total 3 articles about PYRIMIDINE N-OXIDE, 97% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

PYRIMIDINE (289-95-2,25247-63-6) → pyrimidine N-oxide (17043-94-6)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 16h;

DOI:10.1002/anie.200602773

Reference yield: 92.0%

→ pyrimidine N-oxide (17043-94-6)

Guidance literature:

Reference yield:

PYRIMIDINE (289-95-2,25247-63-6) → pyrimidine N-oxide (17043-94-6) + pyrimidine-4(3H)-one (51953-18-5,542-27-8)

Guidance literature:

With dihydrogen peroxide; acetic acid;

DOI:10.1021/jo01105a003

upstream raw materials:

PYRIMIDINE

Downstream raw materials:

1,1,1-trifluoro-N-phenyl-N-(pyrimidin-2-yl)methanesulfonamide

1,1,1-trifluoro-N-phenyl-N-(pyrimidin-4-yl)methanesulfonamide

4-(2,4-pyrimidyl)-1,2,4-triazole

C₆H₅N₅

Refernces

• 1、 Larionov, Oleg V.,Stephens, David,Mfuh, Adelphe M.,Arman, Hadi D.,Naumova, Anastasia S.,Chavez, Gabriel,Skenderi, Behije. "Insights into the mechanistic and synthetic aspects of the Mo/P-catalyzed oxidation of N-heterocycles". . p. 3026 - 3036. Retrieved 2014/05/06.
• 2、 Keith, John M.. "One step conversion of heteroaromatic-N-oxides to imidazolo-heteroarenes". . p. 327 - 330. Retrieved 2008/04/12.