Pd(PPh₃)(CO)

Base Information Edit

Chemical Name:Pd(PPh₃)(CO)
CAS No.:24670-32-4
Molecular Formula:C₅₅H₄₅OP₃Pd
Molecular Weight:921.303
Hs Code.:
Mol file:24670-32-4.mol

Synonyms:Pd(PPh₃)(CO)

Suppliers and Price of Pd(PPh₃)(CO)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Pd(PPh₃)(CO) Edit

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of Pd(PPh₃)(CO)

There total 31 articles about Pd(PPh₃)(CO) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 771476-64-3
trans-[Pd(COEt)(OTs)(PPh₃)₂]

: 201230-82-2
carbon monoxide

: 24670-32-4
Pd(PPh₃)(CO)

Guidance literature:: In methanol; Pd complex treated with CO in MeOH; pptd. with cold H2O; suspn. filtered; ppt. washed with cold H2O; dried (vac.);
DOI:10.1016/j.molcata.2004.04.014

Reference yield: 78.0%

: 201230-82-2
carbon monoxide

: 3375-31-3
palladium diacetate

: 603-35-0
triphenylphosphine

: 24670-32-4
Pd(PPh₃)(CO)

Guidance literature:: In methanol; High Pressure; Pd acetate (0.1 mmol) + PPH3 (0.33 mmol) and MeOH loated in autoclave; purged with CO; pressurized to 5.0 MPa of CO (room temp.); heated (343 K, 30 min, stirring); cooled to room temp.; depressurized; opened; solid filtered off; washed;
DOI:10.1016/j.molcata.2004.04.014

Reference yield: 70.0%

: trans-chloro(methoxycarbonyl)bis(triphenylphosphine)palladium(II)

: 201230-82-2
carbon monoxide

: 1439-36-7
1-triphenylphosphoranylidene-2-propanone

: 24670-32-4
Pd(PPh₃)(CO)

: 616-38-6
carbonic acid dimethyl ester

Guidance literature:: With methanol; In methanol; Pd-compd. suspended in MeOH is pressurized with 40 atm CO at 100°C for 2 h in the presence of PPH3C(H)COCH3 and PPh3; after cooling the suspn. is filtered, residue is identified by IR;
DOI:10.1016/0022-328X(94)88055-7