C₁₈H₁₄Br₄N₂O₅

Base Information

• Chemical Name: C₁₈H₁₄Br₄N₂O₅
• CAS No.: 1446318-10-0
• Molecular Formula: C₁₈H₁₄Br₄N₂O₅
• Molecular Weight: 657.936
• Mol file: 1446318-10-0.mol

Synonyms:C₁₈H₁₄Br₄N₂O₅

Chemical Property of C₁₈H₁₄Br₄N₂O₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₁₈H₁₄Br₄N₂O₅

There total 5 articles about C₁₈H₁₄Br₄N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C18H12Br4N2O4 (1446318-07-5) → C18H14Br4N2O5 (1446318-10-0)

Guidance literature:

C₁₈H₁₂Br₄N₂O₄; With potassium hydroxide; In ethanol; at 20 ℃; for 1h;

With hydrogenchloride; In ethanol;

Reference yield:

2-chloro-4'-ethoxyacetanilide (2153-08-4) → C18H14Br4N2O5 (1446318-10-0)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium iodide; N-benzyl-N,N,N-triethylammonium chloride / 0.17 h / Milling

2: potassium hydroxide / ethanol / 1 h / 20 °C

With N-benzyl-N,N,N-triethylammonium chloride; potassium iodide; potassium hydroxide; In ethanol;

Reference yield:

4-Ethoxyaniline (156-43-4) → C18H14Br4N2O5 (1446318-10-0)

Guidance literature:

Multi-step reaction with 3 steps

1.1: potassium acetate; acetic acid / 0 - 5 °C

1.2: 0.5 h / 20 °C

2.1: potassium iodide; N-benzyl-N,N,N-triethylammonium chloride / 0.17 h / Milling

3.1: potassium hydroxide / ethanol / 1 h / 20 °C

With N-benzyl-N,N,N-triethylammonium chloride; potassium acetate; acetic acid; potassium iodide; potassium hydroxide; In ethanol;

upstream raw materials:

C₁₈H₁₂Br₄N₂O₄

4-Ethoxyaniline

tetrabromophthalimidylacetic acid

Tetrabromophthalic anhydride

Refernces