Technology Process of diethyl 4,4'-dithiobis
There total 10 articles about diethyl 4,4'-dithiobis which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
p-aminoethylbenzoate;
With
tetrafluoroboric acid; sodium nitrite;
In
water; acetone;
at -20 - 0 ℃;
for 0.333333h;
With
carbon disulfide; tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate;
In
acetone;
at 20 ℃;
for 6h;
Irradiation;
DOI:10.3762/bjoc.13.91
- Guidance literature:
-
4-iodobenzoic acid ethyl ester;
With
TurboGrignard;
In
tetrahydrofuran;
at -20 ℃;
for 0.5h;
Schlenk technique;
With
zinc dibromide;
In
tetrahydrofuran;
at -40 ℃;
for 0.5h;
Schlenk technique;
With
disulfur dichloride;
In
tetrahydrofuran;
at -80 ℃;
for 0.166667h;
Schlenk technique;
DOI:10.1021/acs.orglett.8b03319
- Guidance literature:
-
With
sodium hydrogencarbonate;
In
N,N-dimethyl acetamide;
for 120h;
DOI:10.1021/jm00022a015
