3-(4-methoxyphenyl)-5-pentylisoxazole

Base Information

• Chemical Name: 3-(4-methoxyphenyl)-5-pentylisoxazole
• CAS No.: 1592651-35-8
• Molecular Formula: C₁₅H₁₉NO₂
• Molecular Weight: 245.321
• Mol file: 1592651-35-8.mol

Synonyms:3-(4-methoxyphenyl)-5-pentylisoxazole

Chemical Property of 3-(4-methoxyphenyl)-5-pentylisoxazole

Chemical Property:

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Technology Process of 3-(4-methoxyphenyl)-5-pentylisoxazole

There total 1 articles about 3-(4-methoxyphenyl)-5-pentylisoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

1-Heptyne (628-71-7) + N-hydroxy-4-methoxy-benzenecarboximidoyl chloride (38435-51-7) → 3-(4-methoxyphenyl)-5-pentylisoxazole (1592651-35-8)

Guidance literature:

With sodium hydrogencarbonate; In water; isopropyl alcohol; at 20 ℃; for 4h; regioselective reaction;

DOI:10.1007/s13738-013-0307-4

Reference yield: 46.0%

N′-(1-(4-fluorophenyl)ethylidene)-4-methylbenzenesulfonohydrazide (75230-49-8) + 3-(4-methoxyphenyl)-5-pentylisoxazole (1592651-35-8) → 1-(5-(4-fluorophenyl)-2-(4-methoxyphenyl)-1H-pyrrol-3-yl)hexan-1-one

Guidance literature:

With silver hexafluoroantimonate; [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; copper diacetate; In dichloromethane; at 120 ℃; Inert atmosphere; Sealed tube;

DOI:10.1039/d1ob00255d

upstream raw materials:

1-Heptyne

N-hydroxy-4-methoxy-benzenecarboximidoyl chloride

Refernces