C₁₁H₁₂IN

Base Information Edit

Chemical Name:C₁₁H₁₂IN
CAS No.:914299-27-7
Molecular Formula:C₁₁H₁₂IN
Molecular Weight:285.127
Hs Code.:
Mol file:914299-27-7.mol

Synonyms:C₁₁H₁₂IN

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Chemical Property of C₁₁H₁₂IN Edit

Chemical Property:

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Technology Process of C₁₁H₁₂IN

There total 8 articles about C₁₁H₁₂IN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 914299-26-6
C₁₄H₁₄INO₂

: 914299-27-7
C₁₁H₁₂IN

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; water; isopropyl alcohol; at 90 ℃; for 12h;
DOI:10.1016/j.bmcl.2008.09.081

Reference yield:

: 939-83-3
2-cyano-4-nitrotoluene

: 914299-27-7
C₁₁H₁₂IN

Guidance literature:: Multi-step reaction with 7 steps

1.1: hydrogenchloride / dichloromethane; water / 96 h / Heating / reflux

2.1: lithium hydroxide; water / tetrahydrofuran / 4 h / 30 °C

3.1: hydrogen / palladium on activated charcoal / methanol / 3 - 4 h / 40 °C / 2585.81 Torr

4.1: hydrogenchloride; sodium nitrite / water / 1 h / 0 - 30 °C

4.2: 2 h / 0 - 25 °C

5.1: thionyl chloride / 4 h / 0 °C / Heating / reflux

6.1: sodium hydride / tetrahydrofuran / 3 h / Heating / reflux

7.1: hydrogenchloride / tetrahydrofuran; water; isopropyl alcohol / 14 h / Heating / reflux

With hydrogenchloride; lithium hydroxide; thionyl chloride; water; hydrogen; sodium hydride; sodium nitrite; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water; isopropyl alcohol;

Reference yield:

: 7745-93-9
2-bromo-4-nitrotoluene

: 914299-27-7
C₁₁H₁₂IN

Guidance literature:: Multi-step reaction with 8 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 24 h / 80 °C

2.1: hydrogenchloride / dichloromethane; water / 96 h / Heating / reflux

3.1: lithium hydroxide; water / tetrahydrofuran / 4 h / 30 °C

4.1: hydrogen / palladium on activated charcoal / methanol / 3 - 4 h / 40 °C / 2585.81 Torr

5.1: hydrogenchloride; sodium nitrite / water / 1 h / 0 - 30 °C

5.2: 2 h / 0 - 25 °C

6.1: thionyl chloride / 4 h / 0 °C / Heating / reflux

7.1: sodium hydride / tetrahydrofuran / 3 h / Heating / reflux

8.1: hydrogenchloride / tetrahydrofuran; water; isopropyl alcohol / 14 h / Heating / reflux

With hydrogenchloride; lithium hydroxide; thionyl chloride; water; hydrogen; sodium hydride; sodium nitrite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol;