C₁₄H₁₇NO₄

Base Information

• Chemical Name: C₁₄H₁₇NO₄
• CAS No.: 908856-93-9
• Molecular Formula: C₁₄H₁₇NO₄
• Molecular Weight: 263.293
• Mol file: 908856-93-9.mol

Synonyms:C₁₄H₁₇NO₄

Chemical Property of C₁₄H₁₇NO₄

Chemical Property:

Purity/Quality:

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Technology Process of C₁₄H₁₇NO₄

There total 1 articles about C₁₄H₁₇NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

(2S,3R,4S)-4-hydroxyisoleucine (55399-93-4,21704-86-9) + benzyl chloroformate (501-53-1,94274-21-2) → C14H17NO4 (908856-93-9)

Guidance literature:

(2S,3R,4S)-4-hydroxyisoleucine; benzyl chloroformate; With sodium hydroxide; In water; tert-butyl alcohol; at 20 ℃;

With hydrogenchloride; In water; tert-butyl alcohol; pH=2;

Reference yield: 55.0%

pyrrolidine (123-75-1) + C14H17NO4 (908856-93-9) → C19H26N2O4

Guidance literature:

pyrrolidine; C₁₄H₁₇NO₄; In dichloromethane; at 20 ℃; for 6h;

With hydrogenchloride; In dichloromethane; water; ethyl acetate;

Reference yield: 55.0%

pyrrolidine (123-75-1) + C14H17NO4 (908856-93-9) → C19H26N2O4 (908856-94-0)

Guidance literature:

In dichloromethane; at 20 ℃; for 6h;

upstream raw materials:

(2S,3R,4S)-4-hydroxyisoleucine

benzyl chloroformate

Downstream raw materials:

C₁₉H₂₆N₂O₄

Refernces

• 1、 -. "Compounds and compositions for use in the prevention and treatment of obesity and related syndromes". Page/Page column 64. . Retrieved 2010/11/24.