7-ethyl-4-(4-ethylphenyl)-2,3-dibromo-1-naphthyloxyacetyl chloride

Base Information

• Chemical Name: 7-ethyl-4-(4-ethylphenyl)-2,3-dibromo-1-naphthyloxyacetyl chloride
• CAS No.: 80826-24-0
• Molecular Formula: C₂₂H₁₉Br₂ClO₂
• Molecular Weight: 510.653
• Mol file: 80826-24-0.mol

Synonyms:7-ethyl-4-(4-ethylphenyl)-2,3-dibromo-1-naphthyloxyacetyl chloride

Chemical Property of 7-ethyl-4-(4-ethylphenyl)-2,3-dibromo-1-naphthyloxyacetyl chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 7-ethyl-4-(4-ethylphenyl)-2,3-dibromo-1-naphthyloxyacetyl chloride

There total 3 articles about 7-ethyl-4-(4-ethylphenyl)-2,3-dibromo-1-naphthyloxyacetyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[2,3-Dibromo-7-ethyl-4-(4-ethyl-phenyl)-naphthalen-1-yloxy]-acetic acid (80826-08-0) → 7-ethyl-4-(4-ethylphenyl)-2,3-dibromo-1-naphthyloxyacetyl chloride (80826-24-0)

Guidance literature:

With thionyl chloride; N,N-dimethyl-formamide; In benzene; for 4h; Heating;

Reference yield:

[2,3-Dibromo-7-ethyl-4-(4-ethyl-phenyl)-naphthalen-1-yloxy]-acetic acid ethyl ester (80826-07-9) → 7-ethyl-4-(4-ethylphenyl)-2,3-dibromo-1-naphthyloxyacetyl chloride (80826-24-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 70.1 percent / 10percent sodium hydroxide / ethanol / 1 h / Heating

2: thionyl chloride / dimethylformamide / benzene / 4 h / Heating

With sodium hydroxide; thionyl chloride; N,N-dimethyl-formamide; In ethanol; benzene;

Reference yield:

7-ethyl-4-(4-ethylphenyl)-2,3-dibromo-1-naphthol (77379-95-4) → 7-ethyl-4-(4-ethylphenyl)-2,3-dibromo-1-naphthyloxyacetyl chloride (80826-24-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 82.5 percent / sodium ethoxide / ethanol / 3 h / Heating

2: 70.1 percent / 10percent sodium hydroxide / ethanol / 1 h / Heating

3: thionyl chloride / dimethylformamide / benzene / 4 h / Heating

With sodium hydroxide; thionyl chloride; sodium ethanolate; N,N-dimethyl-formamide; In ethanol; benzene;

upstream raw materials:

[2,3-Dibromo-7-ethyl-4-(4-ethyl-phenyl)-naphthalen-1-yloxy]-acetic acid

[2,3-Dibromo-7-ethyl-4-(4-ethyl-phenyl)-naphthalen-1-yloxy]-acetic acid ethyl ester

7-ethyl-4-(4-ethylphenyl)-2,3-dibromo-1-naphthol

Downstream raw materials:

N-Cyclopentyl-2-[2,3-dibromo-7-ethyl-4-(4-ethyl-phenyl)-naphthalen-1-yloxy]-acetamide

N-Butyl-2-[2,3-dibromo-7-ethyl-4-(4-ethyl-phenyl)-naphthalen-1-yloxy]-acetamide

2-[2,3-Dibromo-7-ethyl-4-(4-ethyl-phenyl)-naphthalen-1-yloxy]-acetamide

2-[2,3-Dibromo-7-ethyl-4-(4-ethyl-phenyl)-naphthalen-1-yloxy]-N-isobutyl-acetamide

Refernces