N,N'-dibenzoyl adipic dihydrazide

Base Information

• Chemical Name: N,N'-dibenzoyl adipic dihydrazide
• CAS No.: 35658-33-4
• Molecular Formula: C₂₀H₂₂N₄O₄
• Molecular Weight: 382.419
• Mol file: 35658-33-4.mol

Synonyms:N,N'-dibenzoyl adipic dihydrazide

Chemical Property of N,N'-dibenzoyl adipic dihydrazide

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N'-dibenzoyl adipic dihydrazide

There total 3 articles about N,N'-dibenzoyl adipic dihydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzoic acid hydrazide (613-94-5) + Adipic acid dichloride (111-50-2) → N,N'-dibenzoyl adipic dihydrazide (35658-33-4)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; at 80 ℃; for 2h;

DOI:10.1016/j.polymer.2015.04.062

Reference yield:

benzoyl chloride (98-88-4) + adipic acid dihydrazide (1071-93-8,98152-55-7) → N,N'-dibenzoyl adipic dihydrazide (35658-33-4)

Guidance literature:

With sodium hydroxide;

Reference yield:

diethyl adipate (141-28-6) → N,N'-dibenzoyl adipic dihydrazide (35658-33-4)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrazine hydrate

2: diluted NaOH-solution

With sodium hydroxide; hydrazine hydrate;

upstream raw materials:

benzoyl chloride

adipic acid dihydrazide

diethyl adipate

benzoic acid hydrazide

Downstream raw materials:

bis-(5-phenyl-1,3,4-oxadiazole-2-yl) butane

Refernces

• 1、 Al-Talib, Mahmoud,Tashtoush, Hasan,Odeh, Nedal. "A Convenient Synthesis of Alkyl and Aryl Substituted Bis-1,3,4-oxadiazoles". . p. 1811 - 1817. Retrieved 2007/10/02.