1,3-diphenyl-1,3-dimethoxy propane

Base Information

• Chemical Name: 1,3-diphenyl-1,3-dimethoxy propane
• CAS No.: 26278-69-3
• Molecular Formula: C₁₇H₂₀O₂
• Molecular Weight: 256.345
• Mol file: 26278-69-3.mol

Synonyms:1,3-diphenyl-1,3-dimethoxy propane

Chemical Property of 1,3-diphenyl-1,3-dimethoxy propane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,3-diphenyl-1,3-dimethoxy propane

There total 10 articles about 1,3-diphenyl-1,3-dimethoxy propane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

methanol (67-56-1) + trans-1,2-diphenylcyclopropane (1138-47-2) → 1,3-diphenyl-1,3-dimethoxy propane (26278-69-3)

Guidance literature:

With copper(II) bis(tetrafluoroborate); 9,10-Dicyanoanthracene; In acetonitrile; Irradiation;

DOI:10.1246/cl.1983.941

Reference yield: 75.0%

1,3-diphenyl-1,3-dimethoxy-2-phenylselenenyl propane (116118-10-6) → 1,3-diphenyl-1,3-dimethoxy propane (26278-69-3)

Guidance literature:

nickel; In ethanol;

DOI:10.1016/S0040-4020(01)81734-8

Reference yield: 64.0%

methanol (67-56-1) + cis-1,2-diphenylcyclopropane → 1,3-diphenyl-1,3-dimethoxy propane (26278-69-3)

Guidance literature:

With N-Bromosuccinimide; at 25 ℃; for 48h; regioselective reaction; Inert atmosphere; Darkness;

DOI:10.1002/adsc.201901665

upstream raw materials:

methanol

trans-1,2-diphenylcyclopropane

1,3-diphenyl-1,3-propanediol

1,3-diphenyl-1,3-dimethoxy-2-phenylselenenyl propane

Refernces

• 1、 Tiecco, Marcello,Testaferri, Lorenzo,Tingoli, Marco,Chianelli, Donatella,Bartoli, Donatella. "METHOXYCHLORINATION AND DIMETHOXYLATION OF ALKENES. THE REACTIONS OF SUBSTITUTED STYRENES WITH PHENYLSELENENYL CHLORIDE IN METHANOL". . p. 2261 - 2272. Retrieved 2007/10/02.