7<1H>thioxo-2-phenyl cyclopenta pyridine-6-carbonitrile

Base Information

• Chemical Name: 7<1H>thioxo-2-phenyl cyclopenta pyridine-6-carbonitrile
• CAS No.: 126921-97-9
• Molecular Formula: C₁₅H₁₂N₂S
• Molecular Weight: 252.34
• Mol file: 126921-97-9.mol

Synonyms:7<1H>thioxo-2-phenyl cyclopenta pyridine-6-carbonitrile

Chemical Property of 7<1H>thioxo-2-phenyl cyclopenta pyridine-6-carbonitrile

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 7<1H>thioxo-2-phenyl cyclopenta pyridine-6-carbonitrile

There total 4 articles about 7<1H>thioxo-2-phenyl cyclopenta pyridine-6-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

3-oxo-1-phenyl-3,5,6,7-tetrahydro-2H-cyclopenta[c]pyridine-4-carbonitrile (126921-96-8) → 7<1H>thioxo-2-phenyl cyclopenta pyridine-6-carbonitrile (126921-97-9)

Guidance literature:

With tetraphosphorus decasulfide; In pyridine; for 10h; Heating;

Reference yield:

benzaldehyde (100-52-7) → 7<1H>thioxo-2-phenyl cyclopenta pyridine-6-carbonitrile (126921-97-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 40 percent / ammonium acetate / 5 h / Heating

2: 90 percent / P₂S₅ / pyridine / 10 h / Heating

With ammonium acetate; tetraphosphorus decasulfide; In pyridine;

Reference yield:

ethyl 2-cyano-2-cyclopentylideneacetate (5407-83-0) → 7<1H>thioxo-2-phenyl cyclopenta pyridine-6-carbonitrile (126921-97-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 40 percent / ammonium acetate / 5 h / Heating

2: 90 percent / P₂S₅ / pyridine / 10 h / Heating

With ammonium acetate; tetraphosphorus decasulfide; In pyridine;

upstream raw materials:

3-oxo-1-phenyl-3,5,6,7-tetrahydro-2H-cyclopenta[c]pyridine-4-carbonitrile

ethyl 2-cyano-2-cyclopentylideneacetate

Cyanocarbamidomethylenecyclopentane

benzaldehyde

Downstream raw materials:

7-diethoxycarbonyl methylthio-2-phenyl cyclopenta pyridine-6-carbonitrile

2-(4-Cyano-1-phenyl-6,7-dihydro-5H-[2]pyrindin-3-ylsulfanyl)-N-pyridin-3-yl-acetamide

(4-Cyano-1-phenyl-6,7-dihydro-5H-[2]pyrindin-3-ylsulfanyl)-acetic acid ethyl ester

2-(4-Cyano-1-phenyl-6,7-dihydro-5H-[2]pyrindin-3-ylsulfanyl)-N-phenyl-acetamide

Refernces