Technology Process of 1,7-bis-(4-methoxyphenyl)-heptan-3-one
There total 15 articles about 1,7-bis-(4-methoxyphenyl)-heptan-3-one which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
chloroform;
at 20 ℃;
for 10h;
Inert atmosphere;
DOI:10.1016/j.tet.2013.01.065
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 100 percent / lithium aluminium hydride / diethyl ether
2: 37 percent / phosphorus tribromide / 1.) 0 deg C, 2 h, 2.) room temperature, 4 h
3: 1.) magnesium, 2.) oxalic acid / 1.) ether, 18 h, 2.) water, reflux, 1 h
With
lithium aluminium tetrahydride; oxalic acid; phosphorus tribromide; magnesium;
In
diethyl ether;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 77 percent / aluminium chloride / benzene / 0.5 h / 60 °C
2: 1.) amalgamated zinc, aq. hydrochloric acid, 2.) dimethyl sulphate / 1.) water, toluene, reflux, 24 h, 2.) reflux, 1 h
3: 100 percent / lithium aluminium hydride / diethyl ether
4: 37 percent / phosphorus tribromide / 1.) 0 deg C, 2 h, 2.) room temperature, 4 h
5: 1.) magnesium, 2.) oxalic acid / 1.) ether, 18 h, 2.) water, reflux, 1 h
With
hydrogenchloride; lithium aluminium tetrahydride; aluminium trichloride; amalgamated zinc; oxalic acid; phosphorus tribromide; magnesium; dimethyl sulfate;
In
diethyl ether; benzene;