((1-cyclopropylethoxy)methyl)benzene

Base Information

• Chemical Name: ((1-cyclopropylethoxy)methyl)benzene
• CAS No.: 104948-21-2
• Molecular Formula: C₁₂H₁₆O
• Molecular Weight: 176.258
• Mol file: 104948-21-2.mol

Synonyms:((1-cyclopropylethoxy)methyl)benzene

Chemical Property of ((1-cyclopropylethoxy)methyl)benzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ((1-cyclopropylethoxy)methyl)benzene

There total 1 articles about ((1-cyclopropylethoxy)methyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-cyclopropylethanol (765-42-4) + benzyl bromide (100-39-0) → ((1-cyclopropylethoxy)methyl)benzene (104948-21-2)

Guidance literature:

1-cyclopropylethanol; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.25h; Inert atmosphere;

benzyl bromide; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 2h; Inert atmosphere;

DOI:10.1021/jacs.0c05213

Reference yield: 96.0%

((1-cyclopropylethoxy)methyl)benzene (104948-21-2) → 1-cyclopropylethanol (765-42-4)

Guidance literature:

With ammonia; calcium; In diethyl ether; for 2h; Heating;

DOI:10.1021/jo00374a048

Reference yield: 50.0%

((1-cyclopropylethoxy)methyl)benzene (104948-21-2) + 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane (25015-63-8) → C15H24O + 2-(3-(benzyloxy)-2-methylbutyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:

With iridium(I)-(1,5-cyclooctadiene)-acetylacetonate; (S)-2-<4,5-dihydro-4-(1,1-dimethylethyl)oxazol-2-yl>quinoline; In tetrahydrofuran; at 80 ℃; for 11h; Inert atmosphere; Sealed tube;

DOI:10.1021/jacs.0c05213

upstream raw materials:

1-cyclopropylethanol

benzyl bromide

Downstream raw materials:

1-cyclopropylethanol

Refernces