Technology Process of C32H49BrO4Si
There total 9 articles about C32H49BrO4Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-Bromosuccinimide; sodium carbonate;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 0.833333h;
DOI:10.1021/ja065198n
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: PhLi / tetrahydrofuran; dibutyl ether / 2 h / 20 °C
1.2: 86 percent / tetrahydrofuran; dibutyl ether / -78 - 20 °C
2.1: LiAlH4 / tetrahydrofuran / 2 h / 20 °C
3.1: Et3N / CH2Cl2 / 1.5 h / -60 - 0 °C
4.1: 80.1 g / Dess-Martin periodinane / CH2Cl2 / 0 - 20 °C
5.1: O3 / CH2Cl2 / 5 h / -78 °C
5.2: 99 percent / Zn; AgNO3; AcOH / CH2Cl2 / -78 - 20 °C
6.1: 83 g / NaHMDS / tetrahydrofuran / 0 - 20 °C
7.1: Et3N / CH2Cl2 / 1 h / 0 - 1 °C
8.1: N-bromosuccinimide; Na2CO3 / tetrahydrofuran / 0.83 h / 0 - 20 °C
With
N-Bromosuccinimide; lithium aluminium tetrahydride; sodium hexamethyldisilazane; sodium carbonate; Dess-Martin periodane; ozone; phenyllithium; triethylamine;
In
tetrahydrofuran; dichloromethane; dibutyl ether;
1.2: Wittig reaction / 6.1: Emmons-Wadsworth reaction;
DOI:10.1021/ja065198n
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: O3 / CH2Cl2 / 5 h / -78 °C
1.2: 99 percent / Zn; AgNO3; AcOH / CH2Cl2 / -78 - 20 °C
2.1: 83 g / NaHMDS / tetrahydrofuran / 0 - 20 °C
3.1: Et3N / CH2Cl2 / 1 h / 0 - 1 °C
4.1: N-bromosuccinimide; Na2CO3 / tetrahydrofuran / 0.83 h / 0 - 20 °C
With
N-Bromosuccinimide; sodium hexamethyldisilazane; sodium carbonate; ozone; triethylamine;
In
tetrahydrofuran; dichloromethane;
2.1: Emmons-Wadsworth reaction;
DOI:10.1021/ja065198n
