Technology Process of hydroxymethyl-1 methoxy-4 dimethyl-3,3 cyclohexene-1
There total 4 articles about hydroxymethyl-1 methoxy-4 dimethyl-3,3 cyclohexene-1 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium tetrahydroborate;
In
methanol; water;
for 1h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: NaOAc / aq. acetic acid
2: NaBH4 / methanol; H2O
With
sodium tetrahydroborate; sodium acetate;
In
methanol; water; acetic acid;
DOI:10.1016/S0040-4039(01)95424-3
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 55 percent / boron trifluoride-methanol complex / methanol / 4 h / Heating
2: 61 percent / boron trifluoride etherate / Ambient temperature
3: 95 percent / sodium acetate / acetic acid; H2O / 4 h / Heating
4: 92 percent / NaBH4 / methanol; H2O / 1 h / Ambient temperature
With
sodium tetrahydroborate; boron trifluoride diethyl etherate; sodium acetate; boron trifluoride methanol complex;
In
methanol; water; acetic acid;
