Technology Process of 4-(4-amino-2,6-dibromophenoxy)-2-isopropylphenol
There total 8 articles about 4-(4-amino-2,6-dibromophenoxy)-2-isopropylphenol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
tetrahydrofuran; water; ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium iodide / N,N-dimethyl-formamide / 20 - 100 °C / Inert atmosphere
2: sodium hydroxide / water; N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere
3: boron tribromide / dichloromethane / 0 - 20 °C / Inert atmosphere
4: sodium dithionite / tetrahydrofuran; water / 50 °C / Inert atmosphere
With
sodium dithionite; boron tribromide; sodium iodide; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/acs.jmedchem.6b00173
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydroxide / water; N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere
2: boron tribromide / dichloromethane / 0 - 20 °C / Inert atmosphere
3: sodium dithionite / tetrahydrofuran; water / 50 °C / Inert atmosphere
With
sodium dithionite; boron tribromide; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/acs.jmedchem.6b00173
