benzyl hydrodisulfide

Base Information

• Chemical Name: benzyl hydrodisulfide
• CAS No.: 3492-66-8
• Molecular Formula: C7H8 S2
• Molecular Weight: 156.273
• Hs Code.: 2930909090
• Mol file: 3492-66-8.mol

Synonyms:a-Toluenesulfenic acid, thio-(7CI,8CI); Benzyl hydrodisulfide; Benzyl hydrogen disulfide

Chemical Property of benzyl hydrodisulfide

Chemical Property:

• Vapor Pressure: 0.0706mmHg at 25°C
• Boiling Point: 237°Cat760mmHg
• PKA: 8.37±0.10(Predicted)
• Flash Point: 97.1°C
• PSA: 64.10000
• Density: 1.168g/cm³
• LogP: 2.76460

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of benzyl hydrodisulfide

There total 8 articles about benzyl hydrodisulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetrachloromethane (56-23-5) + 1-chloro-heptadec-8-ene (56554-80-4,123540-84-1) + (N-phenyl-N'-p-tolyl-carbamimidoyl)-thiourea; hydrochloride → dibenzyl sulfide (538-74-9) + benzyl-disulfane (3492-66-8) + N-cyano-N'-phenyl-N''-p-tolyl-guanidine + phenylmethanethiol (100-53-8)

Guidance literature:

Reference yield:

BW-HP-205 → benzyl-disulfane (3492-66-8) + benzaldehyde (100-52-7)

Guidance literature:

With porcine liver esterase; In aq. phosphate buffer; dimethyl sulfoxide; at 37 ℃; for 0.166667h; pH=7.4; Enzymatic reaction;

DOI:10.1002/anie.201704117

Reference yield:

BW-HP-206 → benzyl-disulfane (3492-66-8) + benzaldehyde (100-52-7)

Guidance literature:

With porcine liver esterase; In aq. phosphate buffer; dimethyl sulfoxide; at 37 ℃; for 0.166667h; pH=7.4; Enzymatic reaction;

DOI:10.1002/anie.201704117

upstream raw materials:

tetrachloromethane

1-chloro-heptadec-8-ene

acetyl benzyl disulfide

Downstream raw materials:

2-Benzylthio-4-carboxamidepyridine

dibenzyltrisulfide

methyl 2-(benzyldisulfanyl)acetate

benzyl 2-hydroxyethyl trisulfide

Refernces

• 1、 Chatterji, Tonika,Keerthi, Kripa,Gates, Kent S.. "Generation of reactive oxygen species by a persulfide (BnSSH)". . p. 3921 - 3924. Retrieved 2007/10/03.