3-cyclohexylpropyl caffeate

Base Information

• Chemical Name: 3-cyclohexylpropyl caffeate
• CAS No.: 1240244-46-5
• Molecular Formula: C₁₈H₂₄O₄
• Molecular Weight: 304.386
• Mol file: 1240244-46-5.mol

Synonyms:3-cyclohexylpropyl caffeate

Chemical Property of 3-cyclohexylpropyl caffeate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-cyclohexylpropyl caffeate

There total 6 articles about 3-cyclohexylpropyl caffeate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,5-di-O-caffeoylquinic acid (2450-53-5,16758-05-7,89919-61-9,89919-62-0,101222-97-3) → 3-cyclohexylpropyl caffeate (1240244-46-5)

Guidance literature:

Multi-step reaction with 2 steps

1: Aspergillus japonicus chlorogenate hydrolase immobilized on SEPABEADS EC-QA / 4 h / 40 °C / 760.05 Torr / pH 6.5 / aq. sodium phosphate buffer; Ionic liquid; Enzymatic reaction

2: Candida antarctica lipase B / 24 h / 80 °C / 633.81 Torr / pH 6.5 / aq. sodium phosphate buffer; Ionic liquid; Enzymatic reaction

With Candida antarctica lipase B;

DOI:10.1016/j.molcatb.2011.01.012

Reference yield:

3-cyclohexylpropan-1-ol (1124-63-6) + chlorogenic acid (327-97-9,534-61-2,906-33-2,15016-60-1,15076-00-3,29587-84-6,32719-11-2,72690-58-5,77209-78-0,82659-69-6,82659-70-9,82659-71-0,82690-55-9,93451-45-7,93451-46-8) → caffeic acid (331-39-5,501-16-6) + 3-cyclohexylpropyl caffeate (1240244-46-5)

Guidance literature:

With Aspergillus japonicus chlorogenate hydrolase immobilized on SEPABEADS EC-QA; at 40 ℃; for 10h; under 760.051 Torr; pH=6.5; aq. sodium phosphate buffer; Ionic liquid; Enzymatic reaction;

DOI:10.1016/j.molcatb.2011.01.012

Reference yield:

chlorogenic acid (327-97-9,534-61-2,906-33-2,15016-60-1,15076-00-3,29587-84-6,32719-11-2,72690-58-5,77209-78-0,82659-69-6,82659-70-9,82659-71-0,82690-55-9,93451-45-7,93451-46-8) → 3-cyclohexylpropyl caffeate (1240244-46-5)

Guidance literature:

Multi-step reaction with 2 steps

1: Aspergillus japonicus chlorogenate hydrolase immobilized on SEPABEADS EC-QA / 4 h / 40 °C / 760.05 Torr / pH 6.5 / aq. sodium phosphate buffer; Ionic liquid; Enzymatic reaction

2: Candida antarctica lipase B / 24 h / 80 °C / 633.81 Torr / pH 6.5 / aq. sodium phosphate buffer; Ionic liquid; Enzymatic reaction

With Candida antarctica lipase B;

DOI:10.1016/j.molcatb.2011.01.012

upstream raw materials:

3-cyclohexylpropan-1-ol

chlorogenic acid

neochlorogenic acid

3,5-di-O-caffeoylquinic acid

Refernces