2,2'-(5-Nitro-o-tolylimino)diethanol

Base Information

• Chemical Name: 2,2'-(5-Nitro-o-tolylimino)diethanol
• CAS No.: 21460-74-2
• Molecular Formula: C₁₁H₁₆N₂O₄
• Molecular Weight: 240.259
• Mol file: 21460-74-2.mol

Synonyms:2,2'-(5-Nitro-o-tolylimino)diethanol

Chemical Property of 2,2'-(5-Nitro-o-tolylimino)diethanol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,2'-(5-Nitro-o-tolylimino)diethanol

There total 2 articles about 2,2'-(5-Nitro-o-tolylimino)diethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

oxirane (75-21-8,99932-75-9) + 2-methyl-5-nitroaniline (99-55-8) → 2,2'-(5-Nitro-o-tolylimino)diethanol (21460-74-2)

Guidance literature:

at 150 ℃;

Reference yield:

→ 2,2'-(5-Nitro-o-tolylimino)diethanol (21460-74-2)

Guidance literature:

Aus 2-Amino-4-nitro-toluol;

DOI:10.1021/jm00301a043

Reference yield: 93.0%

2,2'-(5-Nitro-o-tolylimino)diethanol (21460-74-2) → N,N-bis-(2-Chlorethyl)-5-nitro-o-toluidine (21447-45-0)

Guidance literature:

With thionyl chloride; In tetrahydrofuran; benzene; 1) reflux, 2 h; 2) room temperature, 2 d;;

DOI:10.1002/jhet.5570170425

upstream raw materials:

oxirane

2-methyl-5-nitroaniline

Downstream raw materials:

N,N-bis-(2-Chlorethyl)-5-nitro-o-toluidine

3'-<4-(3-Methoxypropyl)-1-piperazinyl>-p-acetotoluidide

1-(2-Methyl-5-nitrophenyl)-4-(3-methoxypropyl)piperazine

1-<3-<4-(3-Methoxypropyl)-1-piperazinyl>-p-tolyl>-3-methylurea