3,6-DiaMino-1,2-dihydro-1,2,4,5-tetrazine Hydrochloride

Base Information

• Chemical Name: 3,6-DiaMino-1,2-dihydro-1,2,4,5-tetrazine Hydrochloride
• CAS No.: 133488-87-6
• Molecular Formula: C₂H₆N₆*ClH
• Molecular Weight: 150.571
• Mol file: 133488-87-6.mol

Synonyms:3,6-diamino-1,2-dihydro-1,2,4,5-tetrazine monohydrochloride

Chemical Property of 3,6-DiaMino-1,2-dihydro-1,2,4,5-tetrazine Hydrochloride

Chemical Property:

• Melting Point: 194-195 °C (decomp)

Purity/Quality:

99% ^*data from raw suppliers

3,6-Diamino-1,2-dihydro-1,2,4,5-tetrazine Hydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 3,6-Diamino-1,2-dihydro-1,2,4,5-tetrazine is the monomer precursor for the synthesis of high metal-complexation linear elastomers containing sym-1,2,4,5-tetrazine rings

Technology Process of 3,6-DiaMino-1,2-dihydro-1,2,4,5-tetrazine Hydrochloride

There total 2 articles about 3,6-DiaMino-1,2-dihydro-1,2,4,5-tetrazine Hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

1,3-diaminoguanidine monohydrochloride (36062-19-8) + acetylacetone (123-54-6,81235-32-7) → 3,5-dimethyl-1H-pyrazole (67-51-6) + 3,6-diamino-1,2-dihydro-1,2,4,5-tetrazine monohydrochloride (133488-87-6)

Guidance literature:

In isopropyl alcohol; 1.) 20 h, ambient temperature, 2.) 8 h, reflux;

Reference yield:

1-aminoamidino-3,5-dimethyl-1H-pyrazole (133488-88-7) → 3,5-dimethyl-1H-pyrazole (67-51-6) + 1,3-diaminoguanidine monohydrochloride (36062-19-8) + 3,6-diamino-1,2-dihydro-1,2,4,5-tetrazine monohydrochloride (133488-87-6) + 3,4,5-triamino-4H-1,2,4-triazole monohydrochloride (1656-15-1,126552-65-6)

Guidance literature:

With sodium hydroxide; In propan-1-ol; Heating;

Reference yield: 100.0%

3,6-diamino-1,2-dihydro-1,2,4,5-tetrazine monohydrochloride (133488-87-6) → 3,6-diamino-1,2,4,5-tetrazine (19617-90-4)

Guidance literature:

With sodium perborate; In water; for 2h; Ambient temperature;

upstream raw materials:

1-aminoamidino-3,5-dimethyl-1H-pyrazole

1,3-diaminoguanidine monohydrochloride

acetylacetone

Downstream raw materials:

3,5-dimethyl-1H-pyrazole

3,5-dimethylpyrazole-1-carboxamide

3,6-diamino-1,2,4,5-tetrazine

Refernces