Diaethyl-m-hydroxybenzylmalonat

Base Information

• Chemical Name: Diaethyl-m-hydroxybenzylmalonat
• CAS No.: 34708-66-2
• Molecular Formula: C₁₄H₁₈O₅
• Molecular Weight: 266.294
• Mol file: 34708-66-2.mol

Synonyms:Diaethyl-m-hydroxybenzylmalonat

Chemical Property of Diaethyl-m-hydroxybenzylmalonat

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of Diaethyl-m-hydroxybenzylmalonat

There total 2 articles about Diaethyl-m-hydroxybenzylmalonat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

m-hydroxybenzyl bromide (74597-04-9) + diethyl malonate (105-53-3) → Diaethyl-m-hydroxybenzylmalonat (34708-66-2)

Guidance literature:

With sodium ethanolate; In ethanol; for 8h; Heating;

DOI:10.1021/jm0001774

Reference yield:

→ Diaethyl-m-hydroxybenzylmalonat (34708-66-2)

Guidance literature:

Diaethyl-m-hydroxybenzylidenmalonat, Hydrierung;

Reference yield:

Diaethyl-m-hydroxybenzylmalonat (34708-66-2) → 2-(3-hydroxy-benzyl)-malonic acid (683215-21-6)

Guidance literature:

With potassium hydroxide; In ethanol; at 0 - 20 ℃; for 4h;

DOI:10.1021/jm0001774

upstream raw materials:

m-hydroxybenzyl bromide

diethyl malonate

Downstream raw materials:

2-(3-hydroxy-benzyl)-malonic acid

Refernces