3,4-dimethyl-2,6-dinitroanisole

Base Information

• Chemical Name: 3,4-dimethyl-2,6-dinitroanisole
• CAS No.: 160754-06-3
• Molecular Formula: C₉H₁₀N₂O₅
• Molecular Weight: 226.189
• Mol file: 160754-06-3.mol

Synonyms:3,4-dimethyl-2,6-dinitroanisole

Chemical Property of 3,4-dimethyl-2,6-dinitroanisole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,4-dimethyl-2,6-dinitroanisole

There total 4 articles about 3,4-dimethyl-2,6-dinitroanisole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

2,6-dinitro-o-xylenol + 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran (96042-30-7) + dimethyl sulfate (77-78-1) → 3,4-dimethyl-2,6-dinitroanisole (160754-06-3)

Guidance literature:

With N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate; In water; acetone;

Reference yield: 93.9%

2,6-dinitro-3,4-dimethylphenol (4097-61-4) + didecyldimethylammonium chloride (7173-51-5) + dimethyl sulfate (77-78-1) → 3,4-dimethyl-2,6-dinitroanisole (160754-06-3)

Guidance literature:

With sodium carbonate; In water; 1,2-dichloro-ethane;

Reference yield: 90.0%

3,4-dimethylanisole (4685-47-6) → 3,4-dimethyl-2,6-dinitroanisole (160754-06-3)

Guidance literature:

3,4-dimethylanisole; With nitric acid; In 1,2-dichloro-ethane; at 20 - 25 ℃; for 5h;

With sulfuric acid; nitric acid; at 55 - 60 ℃; for 5h;

DOI:10.1080/00304940902958669

upstream raw materials:

2,6-dinitro-3,4-dimethylphenol

didecyldimethylammonium chloride

dimethyl sulfate

4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran

Downstream raw materials:

prowl

Refernces

• 1、 -. "Process and intermediate to prepare N-alkyl-3,4-dialkyl-2,6-dinitro-anilines". . . Retrieved 2008/06/13.