2,5-dimethoxyphenyl methyl ketone oxime

Base Information

• Chemical Name: 2,5-dimethoxyphenyl methyl ketone oxime
• CAS No.: 23997-82-2
• Molecular Formula: C₁₀H₁₃NO₃
• Molecular Weight: 195.218
• Mol file: 23997-82-2.mol

Synonyms:2,5-dimethoxyphenyl methyl ketone oxime

Chemical Property of 2,5-dimethoxyphenyl methyl ketone oxime

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,5-dimethoxyphenyl methyl ketone oxime

There total 2 articles about 2,5-dimethoxyphenyl methyl ketone oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2',5'-dimethoxyacetophenone (1201-38-3) → 2,5-dimethoxyphenyl methyl ketone oxime (23997-82-2)

Guidance literature:

With hydroxylamine hydrochloride; sodium acetate; In ethanol; at 80 ℃;

DOI:10.1021/acs.orglett.0c00870

Reference yield:

→ 2,5-dimethoxyphenyl methyl ketone oxime (23997-82-2)

Guidance literature:

DOI:10.1021/ja01221a034

Reference yield: 94.0%

2,5-dimethoxyphenyl methyl ketone oxime (23997-82-2) → 2,5-dimethoxyacetanilide (3467-59-2)

Guidance literature:

With iodine; triphenylphosphine; In acetonitrile; for 0.0833333h; Reflux;

DOI:10.1080/00397911.2011.585270

upstream raw materials:

2',5'-dimethoxyacetophenone

Downstream raw materials:

2-methyl-1,3-benzoxazol-5-ol

5-Methoxy-2-methyl-benzoxazole

2,5-dimethoxyacetanilide

2,5-dimethoxyaniline

Refernces