4-o-tolyloxybutyric acid ethyl ester

Base Information Edit

Chemical Name:4-o-tolyloxybutyric acid ethyl ester
CAS No.:56359-11-6
Molecular Formula:C₁₃H₁₈O₃
Molecular Weight:222.284
Hs Code.:
Mol file:56359-11-6.mol

Synonyms:4-o-tolyloxybutyric acid ethyl ester

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Chemical Property of 4-o-tolyloxybutyric acid ethyl ester Edit

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Technology Process of 4-o-tolyloxybutyric acid ethyl ester

There total 2 articles about 4-o-tolyloxybutyric acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.7%

: 999-10-0
ethyl 4-hydroxybutanoate

: 95-48-7,77504-84-8
ortho-cresol

: 56359-11-6
4-o-tolyloxybutyric acid ethyl ester

Guidance literature:: With Si-Al supported catalyst; at 90 ℃; for 1h;

Reference yield: 69.0%

: 64-17-5
ethanol

: 201230-82-2
carbon monoxide

: 936-72-1
allyl o-tolyl ether

: 56359-11-6
4-o-tolyloxybutyric acid ethyl ester

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2-methyl-but-2-ene; hydrogen; 1,4-di(diphenylphosphino)-butane; In chloroform; at 120 ℃; for 36h; under 31029.7 Torr; regioselective reaction; Schlenk technique; Inert atmosphere; Autoclave;
DOI:10.1021/acs.joc.6b00522