C₃₀H₅₁NO₄S₂Si

Base Information

• Chemical Name: C₃₀H₅₁NO₄S₂Si
• CAS No.: 1426536-09-5
• Molecular Formula: C₃₀H₅₁NO₄S₂Si
• Molecular Weight: 581.957
• Mol file: 1426536-09-5.mol

Synonyms:C₃₀H₅₁NO₄S₂Si

Chemical Property of C₃₀H₅₁NO₄S₂Si

Chemical Property:

Purity/Quality:

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Technology Process of C₃₀H₅₁NO₄S₂Si

There total 5 articles about C₃₀H₅₁NO₄S₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

α-lipoic acid chloride (387358-39-6) + C22H39NO3Si (1426536-08-4) → C30H51NO4S2Si (1426536-09-5)

Guidance literature:

C₂₂H₃₉NO₃Si; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.333333h;

α-lipoic acid chloride; In N,N-dimethyl-formamide; at 20 ℃; for 4h;

Reference yield:

C24H41NO4Si (1426536-06-2) → C30H51NO4S2Si (1426536-09-5)

Guidance literature:

Multi-step reaction with 2 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 14 h / 0 - 60 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 0.33 h / 0 °C

2.2: 4 h / 20 °C

With lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

(R)-1,2-dithiolane-3-pentanoic acid (1200-22-2) → C30H51NO4S2Si (1426536-09-5)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sulfuryl dichloride / benzene / 4 h / 0 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 0.33 h / 0 °C

2.2: 4 h / 20 °C

With sulfuryl dichloride; sodium hydride; In N,N-dimethyl-formamide; benzene;

upstream raw materials:

C₁₈H₂₇NO₄

C₂₄H₄₁NO₄Si

α-lipoic acid chloride

C₂₂H₃₉NO₃Si

Downstream raw materials:

C₂₄H₃₇NO₄S₂

Refernces