3-fluoro-1-formylazulene

Base Information

• Chemical Name: 3-fluoro-1-formylazulene
• CAS No.: 180129-05-9
• Molecular Formula: C₁₁H₇FO
• Molecular Weight: 174.174
• Mol file: 180129-05-9.mol

Synonyms:3-fluoro-1-formylazulene

Chemical Property of 3-fluoro-1-formylazulene

Chemical Property:

Purity/Quality:

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Technology Process of 3-fluoro-1-formylazulene

There total 1 articles about 3-fluoro-1-formylazulene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

N,N-dimethyl-formamide (68-12-2,33513-42-7) + 1-fluoroazulene (67949-59-1) → 3-fluoro-1-formylazulene (180129-05-9)

Guidance literature:

With trichlorophosphate; for 1h; Ambient temperature;

DOI:10.1246/bcsj.69.1645

Reference yield: 55.0%

3-fluoro-1-formylazulene (180129-05-9) → 1-fluoro-3-methylazulene (180129-02-6)

Guidance literature:

With diisobutylaluminium hydride; In diethyl ether; hexane; 1.) -78 deg C, 1 h, 2.) RT, 12 h;

DOI:10.1246/bcsj.69.1645

upstream raw materials:

N,N-dimethyl-formamide

1-fluoroazulene

Downstream raw materials:

1-fluoro-3-methylazulene

Refernces