C₁₈H₁₅ClN₂SSi

Base Information

• Chemical Name: C₁₈H₁₅ClN₂SSi
• CAS No.: 1357109-00-2
• Molecular Formula: C₁₈H₁₅ClN₂SSi
• Molecular Weight: 354.935
• Mol file: 1357109-00-2.mol

Synonyms:C₁₈H₁₅ClN₂SSi

Chemical Property of C₁₈H₁₅ClN₂SSi

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₈H₁₅ClN₂SSi

There total 4 articles about C₁₈H₁₅ClN₂SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

2-{[(pyridin-2-yl)methyl]amino}-benzenethiol (52797-54-3) + Phenyltrichlorosilane (98-13-5) → C18H15ClN2SSi (1357109-00-2)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 20 ℃; for 2.5h; Inert atmosphere;

DOI:10.1039/c1dt11306b

Reference yield:

2-amino-benzenethiol (137-07-5) → C18H15ClN2SSi (1357109-00-2)

Guidance literature:

Multi-step reaction with 3 steps

1: methanol / 3 h / 65 °C

2: methanol; sodium tetrahydroborate / 0 - 65 °C

3: triethylamine / tetrahydrofuran / 2.5 h / 20 °C / Inert atmosphere

With methanol; sodium tetrahydroborate; triethylamine; In tetrahydrofuran; methanol;

DOI:10.1039/c1dt11306b

Reference yield:

pyridine-2-carbaldehyde (1121-60-4) → C18H15ClN2SSi (1357109-00-2)

Guidance literature:

Multi-step reaction with 3 steps

1: methanol / 3 h / 65 °C

2: methanol; sodium tetrahydroborate / 0 - 65 °C

3: triethylamine / tetrahydrofuran / 2.5 h / 20 °C / Inert atmosphere

With methanol; sodium tetrahydroborate; triethylamine; In tetrahydrofuran; methanol;

DOI:10.1039/c1dt11306b

upstream raw materials:

pyridine-2-carbaldehyde

2-{[(pyridin-2-yl)methyl]amino}-benzenethiol

Phenyltrichlorosilane

2-amino-benzenethiol

Downstream raw materials:

C₁₈H₁₅N₅SSi

C₁₉H₁₅N₃S₂Si

C₁₉H₁₅F₃N₂O₃S₂Si

Refernces