Phloroglucinol dihydrate

Base Information

• Chemical Name: Phloroglucinol dihydrate
• CAS No.: 6099-90-7
• Molecular Formula: C6H10O5
• Molecular Weight: 162.142
• Hs Code.: 29072990
• Mol file: 6099-90-7.mol

Synonyms:1,3,5-Benzenetriol,dihydrate (9CI);Phloroglucinol, dihydrate (8CI);1,3,5-Benzènetriol dihydrate;1,3,5-benzenetriol, hydrate (1:2);1,3,5-Benzoltrioldihydrat;Benzene-1,3,5-triol dihydrate;Benzol-1,3,5-trioldihydrat;

Chemical Property of Phloroglucinol dihydrate

Chemical Property:

• Appearance/Colour: off-white powder
• Vapor Pressure: 8.27E-05mmHg at 25°C
• Melting Point: 218-221 °C (A)(lit.)
• Boiling Point: 331.1 °C at 760 mmHg
• Flash Point: 174.9 °C
• PSA: 79.15000
• LogP: 0.67480
• Storage Temp.: Store at RT.
• Sensitive.: Light Sensitive
• Solubility.: Sparingly soluble in water, freely soluble in ethanol (96 per cent), practically insoluble in methylene chloride.
• Water Solubility.: slightly soluble

Purity/Quality:

98%, ^*data from raw suppliers

Phloroglucinol Dihydrate 99+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 37/39-26-36-24/25

MSDS Files:

SDS file from LookChem

Useful:

• Uses: In diazo-type printing, textile dyeing. In cosmetics, as antioxidant; hair colorant. As reagent for detection of aldehydes, carbohydrates including lignin, and HCl. Cloud seeding. Rooting medium for woody plants. Phloroglucinol Dihydrate is a reactant used in the synthesis of [2-13C, 4-13C]-(2R,3S)-catechin and [2-13C, 4-13C]-(2R,3R)-epicatechin.

Technology Process of Phloroglucinol dihydrate

There total 2 articles about Phloroglucinol dihydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

→ 5,7-dihydroxy-3-(2-hydroxyethyl)-4-methyl-2H-1-benzopyran-2-one (155935-98-1) + 1,3,5-Trihydroxybenzene dihydrate (6099-90-7)

Guidance literature:

Reference yield:

→ 1,3,5-Trihydroxybenzene dihydrate (6099-90-7)

Guidance literature:

Reference yield: 100.0%

tetrahydrofuran (109-99-9,24979-97-3,77392-70-2) + 1,1'-bis(ethenyl-4-pyridyl)ferrocene (222165-10-8) + 1,3,5-Trihydroxybenzene dihydrate (6099-90-7) → 1,1'-bis(ethenyl-4-pyridyl)ferrocene phlorglucinol tetrahydrofuran

Guidance literature:

In ethanol; at room temp. for 7 d; elem. anal.;

DOI:10.1002/ejic.200200596

Downstream raw materials:

5,7-dihydroxy-4-propylcoumarin

tribromophloroglucinol triacrylate

3-benzyl-5,7-dihydroxy-4-methyl-2H-chromen-2-one

1,3,5-triacetyl-2,4,6-trihydroxybenzene

Refernces

• 1、 -. "Benzopyranones, processes for their preparation and their use". . . Retrieved 2008/06/13.