24,24-diphenyl 3α,6α-diacetoxy-5β-cholan-23-ene

Base Information Edit

Chemical Name:24,24-diphenyl 3α,6α-diacetoxy-5β-cholan-23-ene
CAS No.:4250-62-8
Molecular Formula:C₄₀H₅₂O₄
Molecular Weight:596.85
Hs Code.:
Mol file:4250-62-8.mol

Synonyms:24,24-diphenyl 3α,6α-diacetoxy-5β-cholan-23-ene

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Chemical Property of 24,24-diphenyl 3α,6α-diacetoxy-5β-cholan-23-ene Edit

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Technology Process of 24,24-diphenyl 3α,6α-diacetoxy-5β-cholan-23-ene

There total 6 articles about 24,24-diphenyl 3α,6α-diacetoxy-5β-cholan-23-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 864-64-2
24,24-diphenyl 3α,6α-dihydroxy-5β-cholan-23-ene

: 108-24-7
acetic anhydride

: 4250-62-8
24,24-diphenyl 3α,6α-diacetoxy-5β-cholan-23-ene

Guidance literature:: With triethylamine; In dichloromethane; for 2h; Reflux;
DOI:10.3390/molecules180910497

Reference yield:

: 4250-63-9
24,24-diphenyl-5β-cholane-3α,6α,24-triol

: 4250-62-8
24,24-diphenyl 3α,6α-diacetoxy-5β-cholan-23-ene

Guidance literature:: Multi-step reaction with 2 steps

1: glacial acetic acid; acetic acid anhydride / Erhitzen des Reaktionsprodukts mit wss.-methanol. NaOH

2: glacial acetic acid

With acetic anhydride; acetic acid;
DOI:10.1021/ja01858a019 DOI:10.1021/ja01213a052

Reference yield:

: phenylmagnesium bromide

: 4250-62-8
24,24-diphenyl 3α,6α-diacetoxy-5β-cholan-23-ene

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / Kochen der vom Aether befreiten Reaktionsloesung

2: glacial acetic acid; acetic acid anhydride / Erhitzen des Reaktionsprodukts mit wss.-methanol. NaOH

3: glacial acetic acid

With acetic anhydride; acetic acid; toluene;
DOI:10.1021/ja01213a052