Technology Process of C23H37O8P
There total 7 articles about C23H37O8P which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
rhodium (II) octanoate dimer;
In
dichloromethane;
at 85 ℃;
for 1h;
Inert atmosphere;
DOI:10.1021/ol3017676
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride / acetonitrile / 21 h / 0 - 20 °C
2: diisobutylaluminium hydride / tetrahydrofuran; dichloromethane / 2 h / -78 °C
3: rhodium (II) octanoate dimer / dichloromethane / 1 h / 85 °C / Inert atmosphere
With
rhodium (II) octanoate dimer; diisobutylaluminium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride;
In
tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/ol3017676
- Guidance literature:
-
Multi-step reaction with 2 steps
1: diisobutylaluminium hydride / tetrahydrofuran; dichloromethane / 2 h / -78 °C
2: rhodium (II) octanoate dimer / dichloromethane / 1 h / 85 °C / Inert atmosphere
With
rhodium (II) octanoate dimer; diisobutylaluminium hydride;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/ol3017676