C₃₀H₃₆O₉

Base Information

• Chemical Name: C₃₀H₃₆O₉
• CAS No.: 1458601-25-6
• Molecular Formula: C₃₀H₃₆O₉
• Molecular Weight: 540.61
• Mol file: 1458601-25-6.mol

Synonyms:C₃₀H₃₆O₉

Chemical Property of C₃₀H₃₆O₉

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₃₀H₃₆O₉

There total 2 articles about C₃₀H₃₆O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

Octanoic acid (124-07-2) + epipodophyllotoxin (4375-07-9) → C30H36O9 (1458601-25-6)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1080/10286020.2018.1490275

Reference yield:

Octanoic acid (124-07-2) + podofilox (518-28-5) → C30H36O9 (1458601-25-6) + C30H36O9

Guidance literature:

With boron trifluoride diethyl etherate; In dichloromethane; at -15 - 20 ℃; for 0.0833333h; Overall yield = 67 percent;

DOI:10.1080/10286020.2018.1490275

Reference yield: 68.0%

C30H36O9 (1458601-25-6) → 2′-chloro-4β-n-octanoyloxypodophyllotoxin (1458601-26-7) + 2′,6′-dichloro-4β-n-octanoyloxypodophyllotoxin (1458601-27-8)

Guidance literature:

With N-chloro-succinimide; In N,N-dimethyl-formamide; at 0 - 60 ℃; for 24h;

DOI:10.1016/j.bmcl.2013.08.044

upstream raw materials:

Octanoic acid

epipodophyllotoxin

podofilox

Downstream raw materials:

2′-chloro-4β-n-octanoyloxypodophyllotoxin

2′,6′-dichloro-4β-n-octanoyloxypodophyllotoxin

Refernces