4-chlorophenyl phenyl oxalate

Base Information

• Chemical Name: 4-chlorophenyl phenyl oxalate
• CAS No.: 96716-00-6
• Molecular Formula: C₁₄H₉ClO₄
• Molecular Weight: 276.676
• Mol file: 96716-00-6.mol

Synonyms:4-chlorophenyl phenyl oxalate

Chemical Property of 4-chlorophenyl phenyl oxalate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-chlorophenyl phenyl oxalate

There total 3 articles about 4-chlorophenyl phenyl oxalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

phenyl oxalyl chloride (51719-70-1) + 4-chloro-phenol (106-48-9,82344-39-6) → 4-chlorophenyl phenyl oxalate (96716-00-6)

Guidance literature:

With triethylamine; In tetrahydrofuran; 1.) 0-5 deg C, 1.5 h, 2.) room temp., 2 h;

DOI:10.1016/S0040-4020(01)81028-0

Reference yield:

oxalyl dichloride (79-37-8) + 4-chloro-phenol (106-48-9,82344-39-6) + phenol (108-95-2,27073-41-2) → 4-chlorophenyl phenyl oxalate (96716-00-6)

Guidance literature:

oxalyl dichloride; phenol; With triethylamine; In benzene;

4-chloro-phenol;

DOI:10.1016/j.jphotochem.2012.12.006

Reference yield:

→ 4-chlorophenyl phenyl oxalate (96716-00-6)

Guidance literature:

Alkoxy-dichlor-essigsaeure-phenylester, 4-Chlor-phenol, Δ;

upstream raw materials:

phenyl oxalyl chloride

4-chloro-phenol

oxalyl dichloride

phenol

Refernces

• 1、 Orosz, Gyoergy. "THE ROLE OF DIARYL OXALATES IN PEROXIOXALATE CHEMILUMINESCENCE". . p. 3493 - 3506. Retrieved 2007/10/02.