trans-1,4-di(phenylcarbonyl)aminocyclohexane-1,4-dinitrile

Base Information

• Chemical Name: trans-1,4-di(phenylcarbonyl)aminocyclohexane-1,4-dinitrile
• CAS No.: 1196087-96-3
• Molecular Formula: C₂₂H₂₀N₄O₂
• Molecular Weight: 372.426
• Mol file: 1196087-96-3.mol

Synonyms:trans-1,4-di(phenylcarbonyl)aminocyclohexane-1,4-dinitrile

Chemical Property of trans-1,4-di(phenylcarbonyl)aminocyclohexane-1,4-dinitrile

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of trans-1,4-di(phenylcarbonyl)aminocyclohexane-1,4-dinitrile

There total 1 articles about trans-1,4-di(phenylcarbonyl)aminocyclohexane-1,4-dinitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

potassium cyanide + benzoyl chloride (98-88-4) + 1,4-Cyclohexanedione (637-88-7) → trans-1,4-di(phenylcarbonyl)aminocyclohexane-1,4-dinitrile (1196087-96-3)

Guidance literature:

potassium cyanide; 1,4-Cyclohexanedione; With ammonium chloride; In water; at 20 ℃; Cooling with ice; Inert atmosphere;

benzoyl chloride; With potassium carbonate; In tetrahydrofuran; water; at 20 ℃; for 72h; Inert atmosphere;

DOI:10.1021/jo901892d

Reference yield: 86.0%

trans-1,4-di(phenylcarbonyl)aminocyclohexane-1,4-dinitrile (1196087-96-3) → trans-1,4-diaminocyclohexane-1,4-dicarboxylic acid dihydrobromide

Guidance literature:

With water; hydrogen bromide; for 96h; Inert atmosphere; Reflux;

DOI:10.1021/jo901892d

upstream raw materials:

benzoyl chloride

1,4-Cyclohexanedione

Refernces