(ethoxy)phenylphosphonodiselenoate sodium salt

Base Information

• Chemical Name: (ethoxy)phenylphosphonodiselenoate sodium salt
• CAS No.: 862075-34-1
• Molecular Formula: C₈H₁₀OPSe₂*Na
• Molecular Weight: 334.05
• Mol file: 862075-34-1.mol

Synonyms:(ethoxy)phenylphosphonodiselenoate sodium salt

Chemical Property of (ethoxy)phenylphosphonodiselenoate sodium salt

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of (ethoxy)phenylphosphonodiselenoate sodium salt

There total 1 articles about (ethoxy)phenylphosphonodiselenoate sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

ethanol (64-17-5) + woollins’ reagent (122039-27-4) → (ethoxy)phenylphosphonodiselenoate sodium salt (862075-34-1)

Guidance literature:

With sodium; at 60 ℃; for 0.25h;

DOI:10.1039/b503793j

Reference yield: 84.0%

(ethoxy)phenylphosphonodiselenoate sodium salt (862075-34-1) + lead(II) acetate trihydrate (6080-56-4) → bis[(ethoxy)phenylphosphonodiselenoato]lead (862075-47-6)

Guidance literature:

In ethanol; N2 atm.; Pb-compound was added to a soln. of phosphinoselenate in ethanol and heated at 50°C for 10 min; ppt. was filtered, washed with methanol, dried in vac.; elem. anal.;

DOI:10.1039/b503793j

Reference yield: 73.0%

(ethoxy)phenylphosphonodiselenoate sodium salt (862075-34-1) + cadmium(II) acetate dihydrate (5743-04-4) → bis[(ethoxy)phenylphosphonodiselenoato]cadmium (862075-39-6)

Guidance literature:

In ethanol; N2 atm.; Cd-salt was added to a soln. of phosphonoselenate in ethanol, heated at 50°C for 10 min; ppt. was filtered, washed with methanol, dried in vac.; elem. anal.;

DOI:10.1039/b503793j

upstream raw materials:

ethanol

woollins’ reagent

Downstream raw materials:

bis[(ethoxy)phenylphosphonodiselenoato]cadmium

bis[(ethoxy)phenylphosphonodiselenoato]lead

Refernces

• 1、 Gray, Ian P.,Slawin, Alexandra M. Z.,Woollins, J. Derek. "Synthesis and structure of novel [Ph(RO)PSe2] complexes". . p. 2188 - 2194. Retrieved 2007/10/03.