perfluoro-(3-piperidinopropionyl fluoride)

Base Information

• Chemical Name: perfluoro-(3-piperidinopropionyl fluoride)
• CAS No.: 17235-58-4
• Molecular Formula: C₈F₁₅NO
• Molecular Weight: 411.07
• Mol file: 17235-58-4.mol

Synonyms:perfluoro-(3-piperidinopropionyl fluoride)

Chemical Property of perfluoro-(3-piperidinopropionyl fluoride)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of perfluoro-(3-piperidinopropionyl fluoride)

There total 7 articles about perfluoro-(3-piperidinopropionyl fluoride) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.7%

methyl 3-(piperidino)propionate (23573-93-5) → perfluoro-(3-piperidinopropionyl fluoride) (17235-58-4) + perfluoro-(1-ethylpiperidine) (564-11-4) + perfluoropentane (678-26-2) + perfluoro(N-methyl-2-methylpyrrolidine) (84940-52-3)

Guidance literature:

With hydrogen fluoride; at 7 - 8 ℃; for 8.93333h; Yield given. Further byproducts given. Title compound not separated from byproducts; electrochemical fluorination;

DOI:10.1016/S0022-1139(00)82821-3

Reference yield: 29.7%

methyl 3-(piperidino)propionate (23573-93-5) → perfluoro-(3-piperidinopropionyl fluoride) (17235-58-4) + perfluoro-(1-ethylpiperidine) (564-11-4) + perfluoropentane (678-26-2) + perfluoro(N-methyl-3-methylpyrrolidine) (84940-44-3)

Guidance literature:

With hydrogen fluoride; at 7 - 8 ℃; for 8.93333h; Yield given. Further byproducts given. Title compound not separated from byproducts; electrochemical fluorination;

DOI:10.1016/S0022-1139(00)82821-3

Reference yield: 29.7%

methyl 3-(piperidino)propionate (23573-93-5) → perfluoro-(3-piperidinopropionyl fluoride) (17235-58-4) + perfluoro-(1-ethylpiperidine) (564-11-4) + perfluoropentane (678-26-2) + perfluoro(N-ethyl-2-methylpyrrolidine)

Guidance literature:

With hydrogen fluoride; at 7 - 8 ℃; for 8.93333h; Yield given. Further byproducts given. Title compound not separated from byproducts; electrochemical fluorination;

DOI:10.1016/S0022-1139(00)82821-3

upstream raw materials:

methyl 3-(piperidino)propionate

Refernces