Ethylenediamine monohydrochloride

Base Information

• Chemical Name: Ethylenediamine monohydrochloride
• CAS No.: 18299-54-2
• Molecular Formula: C2H9ClN2
• Molecular Weight: 96.5599
• European Community (EC) Number: 242-181-0
• NSC Number: 263495,163962
• UNII: 67M1ZLR9SC
• DSSTox Substance ID: DTXSID10885022
• Wikidata: Q27264147
• ChEMBL ID: CHEMBL4085198
• Mol file: 18299-54-2.mol

Synonyms:1,2-diaminoethane;1,2-ethanediamine;edamine;ethane-1,2-diamine;ethyl diamine;ethylenediamine;ethylenediamine (1:1) sulfate;ethylenediamine (1:1) sulfite;ethylenediamine conjugate acid;ethylenediamine dihydrobromide;ethylenediamine dihydrochloride;ethylenediamine dihydrogen iodide;ethylenediamine dihydroiodide;ethylenediamine dinitrate;ethylenediamine hydrochloride;ethylenediamine monohydrochloride;ethylenediamine phosphate;ethylenediamine sulfate;ethylenediamine, 3H-labeled cpd

Chemical Property of Ethylenediamine monohydrochloride

Chemical Property:

• Appearance/Colour: white crystal power with deliquescence property
• Melting Point: 8.5oC
• Boiling Point: 119.7 °C at 760 mmHg
• Flash Point: 33.9 °C
• PSA: 52.04000
• Density: 1.159 g/cm³
• LogP: 1.10640
• Hydrogen Bond Donor Count: 3
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 96.0454260
• Heavy Atom Count: 5
• Complexity: 6

Purity/Quality:

99% ^*data from raw suppliers

2-Aminoethylammoniumchloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C(CN)N.Cl

Technology Process of Ethylenediamine monohydrochloride

There total 5 articles about Ethylenediamine monohydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.8%

chloromethylphosphonic acid (2565-58-4) + ethylenediamine (107-15-3,85404-18-8) → N-(2-aminoethyl)aminomethanephosphonic acid (23575-68-0) + ethylenediamine hydrochloride (18299-54-2)

Guidance literature:

In water; for 20h; Heating;

Reference yield:

N,N′-ethylenebis(3-tert-butylsalicylimine) (72138-54-6) → 3-tert-butyl-2-hydroxybenzaldehyde (24623-65-2) + ethylenediamine hydrochloride (18299-54-2)

Guidance literature:

With hydrogen chloride; In [⁽²⁾H₆]acetone; water; pH=1;

DOI:10.1021/jacs.7b01523

Reference yield:

ethylenediamine (107-15-3,85404-18-8) → ethylenediamine hydrochloride (18299-54-2)

Guidance literature:

With hydrogenchloride;

DOI:10.1039/JR9540002304

upstream raw materials:

1,2-diaminoethane dihydrochloride

chloromethylphosphonic acid

ethylenediamine

N,N′-ethylenebis(3-tert-butylsalicylimine)

Downstream raw materials:

ethylene diurea

piperazine

ethyl 3-(trifluoromethyl)pyrazine-2-carboxylate

C₉H₁₄N₄O₃S

Refernces

• 1、 -. "Synthesis method of saccharide-containing polymeric monomer N-(2-D-glucanoamidoethyl)methacrylamide". Paragraph 0035. . Retrieved 2018/07/30.
• 2、 Cameron, David G.,Hudson, Harry R.,Ojo, Isaac A. O.,Pianka, Max. "ORGANOPHOSPHORUS COMPOUNDS AS POTENTIAL FUNGICIDES. PART I. N-(ω-GUANIDINOALKYL)AMINOALKANEPHOSPHONIC ACIDS AND THEIR AMINOPHOSPHONIC PRECURSORS: PREPARATION, NMR SPECTROSCOPY, AND FAST ATOM BOMBARDMENT MASS SPECTROMETRY". . p. 183 - 198. Retrieved 2007/10/02.