C₆₀H₅₂N₂

Base Information

• Chemical Name: C₆₀H₅₂N₂
• CAS No.: 1610043-94-1
• Molecular Formula: C₆₀H₅₂N₂
• Molecular Weight: 801.086
• Mol file: 1610043-94-1.mol

Synonyms:C₆₀H₅₂N₂

Chemical Property of C₆₀H₅₂N₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₀H₅₂N₂

There total 3 articles about C₆₀H₅₂N₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.5%

3-(4-(N,N-di-(p-tolyl)amino)phenyl)acrylaldehyde (1335233-43-6) + 4,4'-bis(diethoxyphosphinylmethyl)biphenyl (17919-34-5) → C60H52N2 (1610043-94-1)

Guidance literature:

With potassium tert-butylate; In tetrahydrofuran; at 0 ℃; Inert atmosphere;

DOI:10.1039/c4cc01637h

Reference yield:

4-[N,N-di(p-tolyl)amino]benzaldehyde (42906-19-4) → C60H52N2 (1610043-94-1)

Guidance literature:

Multi-step reaction with 3 steps

1.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 °C

1.2: 20 °C

2.1: trichlorophosphate / 0 - 20 °C / Inert atmosphere

3.1: potassium tert-butylate / tetrahydrofuran / 0 °C / Inert atmosphere

With potassium tert-butylate; trichlorophosphate; In tetrahydrofuran; 1.1: |Wittig Olefination / 1.2: |Wittig Olefination / 2.1: |Vilsmeier Reaction / 3.1: |Horner-Wadsworth-Emmons Olefination;

DOI:10.1039/c4cc01637h

Reference yield:

4-methyl-N-p-tolyl-N-(4-vinylphenyl)benzenamine (74065-48-8) → C60H52N2 (1610043-94-1)

Guidance literature:

Multi-step reaction with 2 steps

1: trichlorophosphate / 0 - 20 °C / Inert atmosphere

2: potassium tert-butylate / tetrahydrofuran / 0 °C / Inert atmosphere

With potassium tert-butylate; trichlorophosphate; In tetrahydrofuran; 1: |Vilsmeier Reaction / 2: |Horner-Wadsworth-Emmons Olefination;

DOI:10.1039/c4cc01637h

upstream raw materials:

3-(4-(N,N-di-(p-tolyl)amino)phenyl)acrylaldehyde

4,4'-bis(diethoxyphosphinylmethyl)biphenyl

4-[N,N-di(p-tolyl)amino]benzaldehyde

4-methyl-N-p-tolyl-N-(4-vinylphenyl)benzenamine

Refernces