2-(4-chlorobenzoyl)-1-naphtoic acid

Base Information

• Chemical Name: 2-(4-chlorobenzoyl)-1-naphtoic acid
• CAS No.: 101697-11-4
• Molecular Formula: C₁₈H₁₁ClO₃
• Molecular Weight: 310.737
• Mol file: 101697-11-4.mol

Synonyms:2-(4-chlorobenzoyl)-1-naphtoic acid

Chemical Property of 2-(4-chlorobenzoyl)-1-naphtoic acid

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 2-(4-chlorobenzoyl)-1-naphtoic acid

There total 3 articles about 2-(4-chlorobenzoyl)-1-naphtoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,2-naphthalenedicarboxylic anhydride (5343-99-7) + (4-chlorphenyl)magnesium bromide (873-77-8) → 2-(4-chlorobenzoyl)-1-naphtoic acid (101697-11-4)

Guidance literature:

With diethyl ether; benzene;

DOI:10.1021/ja01270a025

Reference yield:

1,2-naphthalenedicarboxylic anhydride (5343-99-7) + chlorobenzene (108-90-7) → 2-(4-chlorobenzoyl)-1-naphtoic acid (101697-11-4)

Guidance literature:

With aluminium trichloride; sulfuric acid; Yield given. Multistep reaction; 1.) a) 70-75 deg C, 4 h, b) RT, 24 h, 2.) 15 min;

DOI:10.1021/jo00359a058

Reference yield:

1,2-naphthalenedicarboxylic anhydride (5343-99-7) + chlorobenzene (108-90-7) → 2-(4-chlorobenzoyl)-1-naphtoic acid (101697-11-4) + 1-(4-chlorobenzoyl)-2-naphtoic acid (101697-12-5)

Guidance literature:

With aluminium trichloride; Yield given. Multistep reaction. Yields of byproduct given; 1.) 70-75 deg C, 4 h, 2.) RT 24 h;

DOI:10.1021/jo00359a058

upstream raw materials:

1,2-naphthalenedicarboxylic anhydride

(4-chlorphenyl)magnesium bromide

chlorobenzene

Downstream raw materials:

2-(4-chlorophenyl)hydroxymethyl-1-naphtoic acid lactone

2-(4-chlorobenzyl)-1-naphtoic acid

(4-chlorophenyl)(naphthalen-2-yl)methanone

3-(4-chloro-phenyl)-3-methyl-3H-naphtho[1,2-c]furan-1-one

Refernces