2,6-Diethyl-N-(2-propoxyethyl)aniline

Base Information

• Chemical Name: 2,6-Diethyl-N-(2-propoxyethyl)aniline
• CAS No.: 61874-13-3
• Molecular Formula: C₁₅H₂₅NO
• Molecular Weight: 235.37
• Mol file: 61874-13-3.mol

Synonyms:2,6-DIETHYL-N-(2-PROPOXYETHYL)ANILINE;2,6-Diethyl-N-(2-propoxyethyl)-benzenamine;N-Propoxyethyl-2,6-Diethyl Aniline

Chemical Property of 2,6-Diethyl-N-(2-propoxyethyl)aniline

Chemical Property:

• Appearance/Colour: light yellow transparent liquid
• Vapor Pressure: 4.04E-05mmHg at 25°C
• Refractive Index: 1.521
• Boiling Point: 313.9 °C at 760 mmHg
• PKA: 4.01±0.50(Predicted)
• Flash Point: 143.6 °C
• PSA: 21.26000
• Density: 1.896g/cm³
• LogP: 3.72290

Purity/Quality:

99%, ^*data from raw suppliers

2,6-Diethyl-N-(2-propoxyethyl)aniline ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,6-Diethyl-N-(2-propoxyethyl)aniline

There total 6 articles about 2,6-Diethyl-N-(2-propoxyethyl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.9%

2,6-diethylaniline (579-66-8) + 2-chloroethyl propyl ether (42149-74-6) → N-(2-propoxyethyl)-2',6'-diethylaniline (61874-13-3)

Guidance literature:

With N,N-di-n-propyl-2-propoxyethylamine; at 160 ℃; for 10h; Temperature; Reagent/catalyst;

Reference yield: 90.0%

N-(2,6-diethylphenyl)-2-propoxyacetamide → N-(2-propoxyethyl)-2',6'-diethylaniline (61874-13-3)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃; for 8h; Inert atmosphere;

DOI:10.1007/s10593-021-02866-x

Reference yield:

2,6-diethylaniline (579-66-8) + 3-propoxypropionaldehyde (19790-53-5) → N-(2-propoxyethyl)-2',6'-diethylaniline (61874-13-3)

Guidance literature:

With 5%-palladium/activated carbon; hydrogen; acetic acid; In toluene; at 60 - 70 ℃; for 2h; under 22502.3 Torr; Pressure;

upstream raw materials:

2,6-diethylaniline

3-propoxypropionaldehyde

2-chloroethyl propyl ether

2-n-propoxyacetyl chloride

Refernces

• 1、 -. "N, N-di-n-propyl-2-propoxyethylamine as well as preparation method and application thereof". Paragraph 0036-0052. . Retrieved 2020/05/14.