Technology Process of C24H12BrClF2N2OS
There total 6 articles about C24H12BrClF2N2OS which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
toluene;
for 3h;
Reflux;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: catacxium A; palladium diacetate; caesium carbonate / water; toluene / 16 h / 100 °C / Inert atmosphere
2.1: n-butyllithium / tetrahydrofuran / 2 h / -78 °C / Inert atmosphere
2.2: 1 h / -78 - 25 °C
3.1: trifluoroacetic acid / acetonitrile / 1 h / 25 °C
4.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 3 h / Reflux
With
n-butyllithium; palladium diacetate; caesium carbonate; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; catacxium A;
In
tetrahydrofuran; water; toluene; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium / tetrahydrofuran / 2 h / -78 °C / Inert atmosphere
1.2: 1 h / -78 - 25 °C
2.1: trifluoroacetic acid / acetonitrile / 1 h / 25 °C
3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 3 h / Reflux
With
n-butyllithium; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
tetrahydrofuran; toluene; acetonitrile;
