methyl-2-(naphthalen-1-yl)-3-phenylacrylate

Base Information

• Chemical Name: methyl-2-(naphthalen-1-yl)-3-phenylacrylate
• CAS No.: 71432-06-9
• Molecular Formula: C₂₀H₁₆O₂
• Molecular Weight: 288.346
• Mol file: 71432-06-9.mol

Synonyms:methyl-2-(naphthalen-1-yl)-3-phenylacrylate

Chemical Property of methyl-2-(naphthalen-1-yl)-3-phenylacrylate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of methyl-2-(naphthalen-1-yl)-3-phenylacrylate

There total 5 articles about methyl-2-(naphthalen-1-yl)-3-phenylacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 1-naphthylacetate (2876-78-0) + benzaldehyde (100-52-7) → C20H16O2 (71432-06-9) + (Z)-methyl-2-(naphthalen-1-yl)-3-phenylacrylate

Guidance literature:

With sodium methylate; In methanol; at 20 ℃; Reflux; Sealed tube;

DOI:10.1016/j.tetlet.2021.153013

Reference yield:

naphth-1-yl acetic acid (86-87-3) → methyl-2-(naphthalen-1-yl)-3-phenylacrylate (71432-06-9)

Guidance literature:

Multi-step reaction with 2 steps

1: Ac₂O, Et₃N / 160 °C

2: K₂CO₃ / acetone / Heating

With acetic anhydride; potassium carbonate; triethylamine; In acetone;

DOI:10.1021/jm00197a011

Reference yield:

benzaldehyde (100-52-7) → methyl-2-(naphthalen-1-yl)-3-phenylacrylate (71432-06-9)

Guidance literature:

Multi-step reaction with 2 steps

1: Ac₂O, Et₃N / 160 °C

2: K₂CO₃ / acetone / Heating

With acetic anhydride; potassium carbonate; triethylamine; In acetone;

DOI:10.1021/jm00197a011

upstream raw materials:

methyl 1-naphthylacetate

benzaldehyde

naphth-1-yl acetic acid

2-(1-naphthyl)-3-phenylpropenoic acid

Downstream raw materials:

chrysene-5-carboxylic acid methyl ester

Refernces