C₁₉H₂₉⁽²⁾HO₃S

Base Information

• Chemical Name: C₁₉H₂₉⁽²⁾HO₃S
• CAS No.: 208243-27-0
• Molecular Formula: C₁₉H₃₀O₃S
• Molecular Weight: 339.503
• Mol file: 208243-27-0.mol

Synonyms:C₁₉H₂₉⁽²⁾HO₃S

Chemical Property of C₁₉H₂₉⁽²⁾HO₃S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₉H₂₉⁽²⁾HO₃S

There total 3 articles about C₁₉H₂₉⁽²⁾HO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-dodecen-11-one (5009-33-6) → C19H29(2)HO3S (208243-27-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 91 percent / LiAlD₄ / tetrahydrofuran / 1 h / 20 °C

2: DMAP / CH₂Cl₂ / 0.83 h / Heating

With dmap; lithium aluminium deuteride; In tetrahydrofuran; dichloromethane;

DOI:10.1021/ja045475v

Reference yield:

10-Undecenal (112-45-8) → C19H29(2)HO3S (208243-27-0)

Guidance literature:

Multi-step reaction with 4 steps

1: 62 percent / tetrahydrofuran; diethyl ether / 2 h / 0 - 20 °C

2: 84 percent / pyridinium dichromate / CH₂Cl₂ / 3 h / 20 °C

3: 91 percent / LiAlD₄ / tetrahydrofuran / 1 h / 20 °C

4: DMAP / CH₂Cl₂ / 0.83 h / Heating

With dmap; dipyridinium dichromate; lithium aluminium deuteride; In tetrahydrofuran; diethyl ether; dichloromethane;

DOI:10.1021/ja045475v

Reference yield:

10-Undecen-1-ol (112-43-6) → C19H29(2)HO3S (208243-27-0)

Guidance literature:

Multi-step reaction with 5 steps

1: 89 percent / pyridinium chlorochromate / CH₂Cl₂ / 5 h / 20 °C

2: 62 percent / tetrahydrofuran; diethyl ether / 2 h / 0 - 20 °C

3: 84 percent / pyridinium dichromate / CH₂Cl₂ / 3 h / 20 °C

4: 91 percent / LiAlD₄ / tetrahydrofuran / 1 h / 20 °C

5: DMAP / CH₂Cl₂ / 0.83 h / Heating

With dmap; dipyridinium dichromate; lithium aluminium deuteride; pyridinium chlorochromate; In tetrahydrofuran; diethyl ether; dichloromethane;

DOI:10.1021/ja045475v

upstream raw materials:

1-dodecen-11-one

10-Undecenal

10-Undecen-1-ol

Refernces