C₅H₅F₃O₃

Base Information

• Chemical Name: C₅H₅F₃O₃
• CAS No.: 68267-65-2
• Molecular Formula: C₅H₅F₃O₃
• Molecular Weight: 170.088
• Mol file: 68267-65-2.mol

Synonyms:C₅H₅F₃O₃

Chemical Property of C₅H₅F₃O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅H₅F₃O₃

There total 2 articles about C₅H₅F₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethane (74-84-0) + trifluoroacetic anhydride (407-25-0) → 1,1,1-trifluoro-2-butanone (381-88-4) + ethyl trifluoroacetate, (383-63-1) + propionic acid (802294-64-0,79-09-4) + C5H5F3O3 (68267-65-2)

Guidance literature:

With tetraethyllead(IV); at 90 ℃; for 24h; under 51714.8 Torr; Further byproducts given;

DOI:10.1021/ja964068j

Reference yield:

ethane (74-84-0) + trifluoroacetic anhydride (407-25-0) → 1,1,1-trifluoro-2-butanone (381-88-4) + acetic acid (64-19-7,77671-22-8) + propionic acid (802294-64-0,79-09-4) + C5H5F3O3 (68267-65-2)

Guidance literature:

With ethene; dihydrogen peroxide; In water; at 75 - 80 ℃; for 24h; under 51714.8 Torr; Further byproducts given;

DOI:10.1021/ja964068j

Reference yield:

n-butanethiol (109-79-5) + C5H5F3O3 (68267-65-2) → butyl thiopropionate (2432-44-2)

Guidance literature:

In dichloromethane; for 4h; Yield given; Heating;

upstream raw materials:

ethane

trifluoroacetic anhydride

Downstream raw materials:

butyl thiopropionate

Refernces