methanesulfonic acid p-phenetidide

Base Information

• Chemical Name: methanesulfonic acid p-phenetidide
• CAS No.: 10406-66-3
• Molecular Formula: C₉H₁₃NO₃S
• Molecular Weight: 215.273
• Mol file: 10406-66-3.mol

Synonyms:methanesulfonic acid p-phenetidide

Chemical Property of methanesulfonic acid p-phenetidide

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of methanesulfonic acid p-phenetidide

There total 2 articles about methanesulfonic acid p-phenetidide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

N-(4-oxocyclohexa-2,5-dien-1-ylidene)methanesulphonamide (73021-84-8) + triethyl phosphite (122-52-1) → methanesulfonic acid p-phenetidide (10406-66-3) + 4-(methylsulfonylamino)phenol (51767-39-6) + N-(4-Ethoxy-phenyl)-N-ethyl-methanesulfonamide

Guidance literature:

In benzene; for 4h; Ambient temperature;

Reference yield:

→ methanesulfonic acid p-phenetidide (10406-66-3)

Guidance literature:

Geschwindigkeit der B. bei 19grad u. 80grad;

Reference yield: 86.0%

methanesulfonic acid p-phenetidide (10406-66-3) → Phenetole (103-73-1)

Guidance literature:

With chloroamine; sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃;

DOI:10.1021/jo010681w

upstream raw materials:

N-(4-oxocyclohexa-2,5-dien-1-ylidene)methanesulphonamide

triethyl phosphite

Downstream raw materials:

methanesulfonic acid-(4-ethoxy-2-nitro-anilide)

methanesulfonic acid-(4-ethoxy-2,6-dinitro-anilide)

Phenetole

2-nitro-4-ethoxyaniline

Refernces