methyl-(2-methyl-benzyl)-sulfone

Base Information

• Chemical Name: methyl-(2-methyl-benzyl)-sulfone
• CAS No.: 261924-13-4
• Molecular Formula: C₉H₁₂O₂S
• Molecular Weight: 184.259
• Mol file: 261924-13-4.mol

Synonyms:methyl-(2-methyl-benzyl)-sulfone

Chemical Property of methyl-(2-methyl-benzyl)-sulfone

Chemical Property:

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of methyl-(2-methyl-benzyl)-sulfone

There total 11 articles about methyl-(2-methyl-benzyl)-sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-methyl-2-<(methylthio)methyl>benzene (5925-79-1) → methyl-(2-methyl-benzyl)-sulfone (261924-13-4)

Guidance literature:

With dihydrogen peroxide; acetic acid;

DOI:10.1021/ja01107a032

Reference yield:

[(methylthio)methyl]-benzene (766-92-7) → methyl-(2-methyl-benzyl)-sulfone (261924-13-4)

Guidance literature:

Multi-step reaction with 3 steps

1: KNH₂; liquid NH₃ / Erwaermen des mit Aether versetzten Reaktionsgemisches

2: aqueous NaOH

3: aqueous H₂O₂; acetic acid

With sodium hydroxide; ammonia; dihydrogen peroxide; potassium amide; acetic acid;

DOI:10.1021/ja01107a032

Reference yield:

2-methylbenzyl mercaptan (7341-24-4) → methyl-(2-methyl-benzyl)-sulfone (261924-13-4)

Guidance literature:

Multi-step reaction with 2 steps

1: aqueous NaOH

2: aqueous H₂O₂; acetic acid

With sodium hydroxide; dihydrogen peroxide; acetic acid;

DOI:10.1021/ja01107a032

upstream raw materials:

1-methyl-2-<(methylthio)methyl>benzene

[(methylthio)methyl]-benzene

2-methylbenzyl mercaptan

S-benzyldimethylsulfonium bromide

Refernces

• 1、 -. "Azetidine derivatives, their preparation and medicaments containing them". . . Retrieved 2008/06/13.